Literature DB >> 20203411

(E)-N-{[6-chloro-4-(4-chlorophenyl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridin-5-yl]methylene}benzene-1,2-diamine: a three-dimensional framework structure built from only two hydrogen bonds.

Yurina Díaz1, Jairo Quiroga, Justo Cobo, Christopher Glidewell.   

Abstract

The molecules of the title compound, C(26)H(19)Cl(2)N(5), are conformationally chiral, with none of the aryl groups coplanar with the pyrazolo[3,4-b]pyridine core of the molecule. A single unique N-H...N hydrogen bond links the molecules into two symmetry-related sets of C(11) chains running parallel to the [011] and [011] directions, respectively, and these two sets of chains are linked into a continuous three-dimensional framework structure by a single unique C-H...N hydrogen bond which forms a chain parallel to the [100] direction.

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Year:  2010        PMID: 20203411      PMCID: PMC2855570          DOI: 10.1107/S0108270110004026

Source DB:  PubMed          Journal:  Acta Crystallogr C        ISSN: 0108-2701            Impact factor:   1.172


  8 in total

1.  C-H...pi and pi--pi interactions in the supramolecular structure of 3-methyl-1,4-diphenyl-1H-pyrazolo[3,4-b]pyridine.

Authors:  John N Low; Justo Cobo; Manuel Nogueras; Adolfo Sánchez; Harlen Torres; Braulio Insuasty
Journal:  Acta Crystallogr C       Date:  2002-04-30       Impact factor: 1.172

2.  The Cambridge Structural Database: a quarter of a million crystal structures and rising.

Authors:  Frank H Allen
Journal:  Acta Crystallogr B       Date:  2002-05-29

3.  N-benzylethylammonium nitrate: a three-dimensional hydrogen-bonded framework comprising substructures in zero, one and two dimensions.

Authors:  Rodrigo Abonia; Emerson Rengifo; Justo Cobo; John N Low; Christopher Glidewell
Journal:  Acta Crystallogr C       Date:  2005-10-22       Impact factor: 1.172

4.  A short history of SHELX.

Authors:  George M Sheldrick
Journal:  Acta Crystallogr A       Date:  2007-12-21       Impact factor: 2.290

5.  Supramolecular aggregation in three 4-aryl-6-(1H-indol-3-yl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carbonitriles.

Authors:  John N Low; Justo Cobo; Ana Sánchez; Jorge Trilleras; Christopher Glidewell
Journal:  Acta Crystallogr C       Date:  2007-04-14       Impact factor: 1.172

6.  4-(2-Fluorophenyl)-6-(1H-indol-1-yl)-3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carbonitrile: a chain of rings built from N-H...N, C-H...N and C-H...pi(arene) hydrogen bonds.

Authors:  Jairo Quiroga; Ana Sánchez; Justo Cobo; Christopher Glidewell
Journal:  Acta Crystallogr C       Date:  2009-07-09       Impact factor: 1.172

7.  Determination of absolute structure using Bayesian statistics on Bijvoet differences.

Authors:  Rob W W Hooft; Leo H Straver; Anthony L Spek
Journal:  J Appl Crystallogr       Date:  2008-01-16       Impact factor: 3.304

8.  Structure validation in chemical crystallography.

Authors:  Anthony L Spek
Journal:  Acta Crystallogr D Biol Crystallogr       Date:  2009-01-20
  8 in total

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