Literature DB >> 20059126

Solid and liquid spectroscopic analysis (SALSA)--a soft x-ray spectroscopy endstation with a novel flow-through liquid cell.

M Blum1, L Weinhardt, O Fuchs, M Bär, Y Zhang, M Weigand, S Krause, S Pookpanratana, T Hofmann, W Yang, J D Denlinger, E Umbach, C Heske.   

Abstract

We present a novel synchrotron endstation with a flow-through liquid cell designed to study the electronic structure of liquids using soft x-ray spectroscopies. In this cell, the liquid under study is separated from the vacuum by a thin window membrane, such that the sample liquid can be investigated at ambient pressure. The temperature of the probing volume can be varied in a broad range and with a fast temperature response. The optimized design of the cell significantly reduces the amount of required sample liquid and allows the use of different window membrane types necessary to cover a broad energy range. The liquid cell is integrated into the solid and liquid spectroscopic analysis (SALSA) endstation that includes a high-resolution, high-transmission x-ray spectrometer and a state-of-the-art electron analyzer. The modular design of SALSA also allows the measurement of solid-state samples. The capabilities of the liquid cell and the x-ray spectrometer are demonstrated using a resonant inelastic x-ray scattering map of a 25 wt % NaOD solution.

Entities:  

Year:  2009        PMID: 20059126     DOI: 10.1063/1.3257926

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  5 in total

1.  Elemental-sensitive Detection of the Chemistry in Batteries through Soft X-ray Absorption Spectroscopy and Resonant Inelastic X-ray Scattering.

Authors:  Jinpeng Wu; Shawn Sallis; Ruimin Qiao; Qinghao Li; Zengqing Zhuo; Kehua Dai; Zixuan Guo; Wanli Yang
Journal:  J Vis Exp       Date:  2018-04-17       Impact factor: 1.355

2.  X-SPEC: a 70 eV to 15 keV undulator beamline for X-ray and electron spectroscopies.

Authors:  Lothar Weinhardt; Ralph Steininger; Dagmar Kreikemeyer-Lorenzo; Stefan Mangold; Dirk Hauschild; David Batchelor; Thomas Spangenberg; Clemens Heske
Journal:  J Synchrotron Radiat       Date:  2021-02-10       Impact factor: 2.616

3.  Opportunities and challenges of applying advanced X-ray spectroscopy to actinide and lanthanide N-donor ligand systems.

Authors:  Tim Pruessmann; Peter Nagel; Laura Simonelli; David Batchelor; Robert Gordon; Bernd Schimmelpfennig; Michael Trumm; Tonya Vitova
Journal:  J Synchrotron Radiat       Date:  2022-01-01       Impact factor: 2.616

4.  Steep sulfur gradient in CZTSSe solar cells by H2S-assisted rapid surface sulfurization.

Authors:  Teoman Taskesen; Devendra Pareek; Dirk Hauschild; Alan Haertel; Lothar Weinhardt; Wanli Yang; Timo Pfeiffelmann; David Nowak; Clemens Heske; Levent Gütay
Journal:  RSC Adv       Date:  2021-04-01       Impact factor: 3.361

5.  Semitransparent Sb2S3 thin film solar cells by ultrasonic spray pyrolysis for use in solar windows.

Authors:  Jako S Eensalu; Atanas Katerski; Erki Kärber; Lothar Weinhardt; Monika Blum; Clemens Heske; Wanli Yang; Ilona Oja Acik; Malle Krunks
Journal:  Beilstein J Nanotechnol       Date:  2019-12-06       Impact factor: 3.649

  5 in total

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