Literature DB >> 19947620

2D ultrafast HMBC: a valuable tool for monitoring organic reactions.

Antonio Herrera1, Encarnación Fernández-Valle, Eva M Gutiérrez, Roberto Martínez-Alvarez, Dolores Molero, Zulay D Pardo, Elena Sáez.   

Abstract

Ultrafast 2D HMBC spectroscopy permits real-time monitoring of a reaction based on the structural changes produced in a carbonyl carbon atom. This new technique was used to study the reaction of ketones, nitriles, and Tf(2)O, affording relevant information about new intermediates and kinetic data.

Entities:  

Year:  2010        PMID： 19947620     DOI： 10.1021/ol902532f

Source DB:  PubMed          Journal:  Org Lett        ISSN： 1523-7052            Impact factor:   6.005


  2 in total

1.  Monitoring mechanistic details in the synthesis of pyrimidines via real-time, ultrafast multidimensional NMR spectroscopy.

Authors:  Zulay D Pardo; Gregory L Olsen; María Encarnación Fernández-Valle; Lucio Frydman; Roberto Martínez-Álvarez; Antonio Herrera
Journal:  J Am Chem Soc       Date:  2012-01-27       Impact factor: 15.419

Review 2.  Ultrafast 2D NMR: an emerging tool in analytical spectroscopy.

Authors:  Patrick Giraudeau; Lucio Frydman
Journal:  Annu Rev Anal Chem (Palo Alto Calif)       Date:  2014       Impact factor: 10.745
  2 in total

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