Literature DB >> 19757483

Constant time gradient HSQC-iDOSY: practical aspects.

A S McLachlan1, J J Richards, A R Bilia, G A Morris.   

Abstract

An improved constant time gradient HSQC-iDOSY pulse sequence is presented, and the corresponding form of the Stejskal-Tanner equation is derived. The pulse sequence is particularly well suited to the problem of analysing mixtures of chemically cognate species, where the high spectral resolution afforded by 1H-13C correlation methods is needed for DOSY experiments to give good diffusion resolution. Its use is illustrated for a mixture of rutin and its aglycone quercetin. Copyright 2009 John Wiley & Sons, Ltd.

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Year:  2009        PMID: 19757483     DOI: 10.1002/mrc.2518

Source DB:  PubMed          Journal:  Magn Reson Chem        ISSN: 0749-1581            Impact factor:   2.447


  2 in total

1.  Methods to determine slow diffusion coefficients of biomolecules: applications to Engrailed 2, a partially disordered protein.

Authors:  Rafal Augustyniak; Fabien Ferrage; Raphaël Paquin; Olivier Lequin; Geoffrey Bodenhausen
Journal:  J Biomol NMR       Date:  2011-05-21       Impact factor: 2.835

2.  Measuring translational diffusion coefficients of peptides and proteins by PFG-NMR using band-selective RF pulses.

Authors:  Shenggen Yao; Daniel K Weber; Frances Separovic; David W Keizer
Journal:  Eur Biophys J       Date:  2014-05-14       Impact factor: 1.733

  2 in total

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