Literature DB >> 19601681

Preparation and crystal growth of Na24Si136.

Matt Beekman1, Michael Baitinger, Horst Borrmann, Walter Schnelle, Katrin Meier, George S Nolas, Yuri Grin.   

Abstract

The synthesis and single crystal growth of clathrate-II Na(24)Si(136) is performed in one step applying the spark plasma treatment to the precursor Na(4)Si(4). The reported results demonstrate a new route to intermetallic compounds facilitated by the electric field and current. SPS is revealed to offer significant opportunities as a novel preparatory method for synthesis and crystal growth of solid state materials.

Entities:  

Year:  2009        PMID： 19601681     DOI： 10.1021/ja903362b

Source DB:  PubMed          Journal:  J Am Chem Soc        ISSN： 0002-7863            Impact factor:   15.419


  5 in total

1.  Binary Alkali-Metal Silicon Clathrates by Spark Plasma Sintering: Preparation and Characterization.

Authors:  Igor Veremchuk; Matt Beekman; Iryna Antonyshyn; Walter Schnelle; Michael Baitinger; George S Nolas; Yuri Grin
Journal:  Materials (Basel)       Date:  2016-07-19       Impact factor: 3.623

2.  Structure and Transport Properties of Dense Polycrystalline Clathrate-II (K,Ba)16(Ga,Sn)136 Synthesized by a New Approach Employing SPS.

Authors:  Kaya Wei; Xiaoyu Zeng; Terry M Tritt; Artem R Khabibullin; Lilia M Woods; George S Nolas
Journal:  Materials (Basel)       Date:  2016-08-26       Impact factor: 3.623

3.  On the Role of the Electrical Field in Spark Plasma Sintering of UO2+x.

Authors:  Vaclav Tyrpekl; Mohamed Naji; Michael Holzhäuser; Daniel Freis; Damien Prieur; Philippe Martin; Bert Cremer; Mairead Murray-Farthing; Marco Cologna
Journal:  Sci Rep       Date:  2017-04-19       Impact factor: 4.379

4.  Na-Ga-Si type-I clathrate single crystals grown via Na evaporation using Na-Ga and Na-Ga-Sn fluxes.

Authors:  Hironao Urushiyama; Haruhiko Morito; Hisanori Yamane; Masami Terauchi
Journal:  RSC Adv       Date:  2018-12-04       Impact factor: 4.036

5.  In-Cage Interactions in the Clathrate Superconductor Sr8 Si46.

Authors:  Julia-Maria Hübner; Yurii Prots; Walter Schnelle; Matej Bobnar; Markus König; Michael Baitinger; Paul Simon; Wilder Carrillo-Cabrera; Alim Ormeci; Eteri Svanidze; Yuri Grin; Ulrich Schwarz
Journal:  Chemistry       Date:  2019-12-12       Impact factor: 5.236
  5 in total

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