| Literature DB >> 19572259 |
Maria Misiak1, Wiktor Koźmiński, Maria Kwasiborska, Jacek Wójcik, Ewa Ciepichal, Ewa Swiezewska.
Abstract
The complete assignment of (1)H and (13)C chemical shifts of natural abundance prenol-10 is reported for the first time. It was achieved using 3D NMR experiments, which were based on random sampling of the evolution time space followed by multidimensional Fourier transform. This approach makes it possible to acquire 3D NMR spectra in a reasonable time and preserves high resolution in indirectly detected dimensions. It is shown that the interpretation of 3D COSY-HMBC and 3D TOCSY-HSQC spectra is crucial in the structural analysis of prenol-10. Copyright (c) 2009 John Wiley & Sons, Ltd.Mesh：
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Year: 2009 PMID： 19572259 DOI： 10.1002/mrc.2473
Source DB: PubMed Journal: Magn Reson Chem ISSN： 0749-1581 Impact factor: 2.447