Literature DB >> 19422194

Microflow radical carboaminoxylations with a novel alkoxyamine.

Inga C Wienhöfer1, Armido Studer, Md Taifur Rahman, Takahide Fukuyama, Ilhyong Ryu.   

Abstract

Highly efficient thermal radical carboaminoxylations of various olefins by using the novel alkoxyamine A to give adducts of type B are described. It is reported that these radical addition reactions can be performed in a microflow reaction system. As compared to conventional batch reaction setup, significantly higher yields are obtained by running carboaminoxylations using the microflow system under analogous conditions.

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Year:  2009        PMID: 19422194     DOI: 10.1021/ol900713d

Source DB:  PubMed          Journal:  Org Lett        ISSN: 1523-7052            Impact factor:   6.005


  5 in total

1.  Nature-inspired total synthesis of (-)-fusarisetin A.

Authors:  Jing Xu; Eduardo J E Caro-Diaz; Lynnie Trzoss; Emmanuel A Theodorakis
Journal:  J Am Chem Soc       Date:  2012-03-08       Impact factor: 15.419

2.  Fusarisetin A: Scalable Total Synthesis and Related Studies.

Authors:  Jing Xu; Eduardo J E Caro-Diaz; Michelle H Lacoske; Chao-I Hung; Colin Jamora; Emmanuel A Theodorakis
Journal:  Chem Sci       Date:  2012-08-23       Impact factor: 9.825

3.  Koch-Haaf reaction of adamantanols in an acid-tolerant hastelloy-made microreactor.

Authors:  Takahide Fukuyama; Yu Mukai; Ilhyong Ryu
Journal:  Beilstein J Org Chem       Date:  2011-09-15       Impact factor: 2.883

4.  Translation of microwave methodology to continuous flow for the efficient synthesis of diaryl ethers via a base-mediated S(N)Ar reaction.

Authors:  Charlotte Wiles; Paul Watts
Journal:  Beilstein J Org Chem       Date:  2011-10-04       Impact factor: 2.883

5.  Flow Giese reaction using cyanoborohydride as a radical mediator.

Authors:  Takahide Fukuyama; Takuji Kawamoto; Mikako Kobayashi; Ilhyong Ryu
Journal:  Beilstein J Org Chem       Date:  2013-09-03       Impact factor: 2.883

  5 in total

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