Literature DB >> 19410491

High-resolution 1H homonuclear dipolar recoupling NMR spectra of biological solids at MAS rates up to 67 kHz.

Luis Mafra1, Renée Siegel, Christian Fernandez, Denis Schneider, Fabien Aussenac, João Rocha.   

Abstract

Two-dimensional (1)H homonuclear correlation NMR spectra of solids of biological interest have been recorded at high magnetic fields (14.1 and 18.8 T) and MAS rates up to 67 kHz, using RN(n)(nu) symmetry-based homonuclear recoupling and CRAMPS decoupling; this method affords exceptional spectral resolution and is well suited to probe (1)H-(1)H proximities in powdered solids.

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Year:  2009        PMID: 19410491     DOI: 10.1016/j.jmr.2009.04.004

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  2 in total

1.  Proton-detected heteronuclear single quantum correlation NMR spectroscopy in rigid solids with ultra-fast MAS.

Authors:  Gregory P Holland; Brian R Cherry; Janelle E Jenkins; Jeffery L Yarger
Journal:  J Magn Reson       Date:  2009-10-04       Impact factor: 2.229

2.  Acidity enhancement through synergy of penta- and tetra-coordinated aluminum species in amorphous silica networks.

Authors:  Zichun Wang; Tong Li; Yijiao Jiang; Olivier Lafon; Zongwen Liu; Julien Trébosc; Alfons Baiker; Jean-Paul Amoureux; Jun Huang
Journal:  Nat Commun       Date:  2020-01-13       Impact factor: 14.919

  2 in total

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