Literature DB >> 19101127

Homonuclear dipolar decoupling schemes for fast MAS.

Jean-Paul Amoureux1, Bingwen Hu, Julien Trébosc, Qiang Wang, Olivier Lafon, Feng Deng.   

Abstract

We present two one-dimensional methods that allow direct observation of highly resolved (1)H spectra in solid-state NMR. The methods, which work mainly at 30-35kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.

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Year:  2008        PMID: 19101127     DOI: 10.1016/j.ssnmr.2008.10.006

Source DB:  PubMed          Journal:  Solid State Nucl Magn Reson        ISSN: 0926-2040            Impact factor:   2.293


  1 in total

1.  Optimisation of 1H PMLG homonuclear decoupling at 60 kHz MAS to enable 15N-1H through-bond heteronuclear correlation solid-state NMR spectroscopy.

Authors:  Jacqueline Tognetti; W Trent Franks; Józef R Lewandowski; Steven P Brown
Journal:  Phys Chem Chem Phys       Date:  2022-08-31       Impact factor: 3.945

  1 in total

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