Literature DB >> 19019378

Simultaneous extraction and clean-up of polychlorinated biphenyls and their metabolites from small tissue samples using pressurized liquid extraction.

Izabela Kania-Korwel1, Hongxia Zhao, Karin Norstrom, Xueshu Li, Keri C Hornbuckle, Hans-Joachim Lehmler.   

Abstract

A pressurized liquid extraction-based method for the simultaneous extraction and in situ clean-up of polychlorinated biphenyls (PCBs), hydroxylated (OH)-PCBs and methylsulfonyl (MeSO(2))-PCBs from small (<0.5 g) tissue samples was developed and validated. Extraction of a laboratory reference material with hexane-dichloromethane-methanol (48:43:9, v/v) and Florisil as fat retainer allowed an efficient recovery of PCBs (78-112%; RSD: 13-37%), OH-PCBs (46+/-2%; RSD: 4%) and MeSO(2)-PCBs (89+/-21%; RSD: 24%). Comparable results were obtained with an established analysis method for PCBs, OH-PCBs and MeSO(2)-PCBs.

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Year:  2008        PMID： 19019378      PMCID： PMC2648864          DOI： 10.1016/j.chroma.2008.10.089

Source DB:  PubMed          Journal:  J Chromatogr A        ISSN： 0021-9673            Impact factor:   4.759


  44 in total

1.  Extraction and cleanup methods for analysis of phenolic and neutral organohalogens in plasma.

Authors:  L Hovander; M Athanasiadou; L Asplund; S Jensen; E K Wehler
Journal:  J Anal Toxicol       Date:  2000 Nov-Dec       Impact factor: 3.367

2.  Sediment certified reference materials for the determination of polychlorinated biphenyls and organochlorine pesticides from the National Metrology Institute of Japan (NMIJ).

Authors:  Masahiko Numata; Takashi Yarita; Yoshie Aoyagi; Yoko Tsuda; Misako Yamazaki; Akiko Takatsu; Keiichiro Ishikawa; Koichi Chiba; Kensaku Okamaoto
Journal:  Anal Bioanal Chem       Date:  2006-09-22       Impact factor: 4.142

3.  Enantioselective formation of methyl sulfone metabolites of 2,2',3,3',4,6'-hexachlorobiphenyl in rat.

Authors:  Karin Norstrom; Johan Eriksson; Johanna Haglund; Virginia Silvari; Ake Bergman
Journal:  Environ Sci Technol       Date:  2006-12-15       Impact factor: 9.028

4.  Dose-dependent enantiomeric enrichment of 2,2',3,3',6,6'-hexachlorobiphenyl in female mice.

Authors:  Izabela Kania-Korwel; Keri C Hornbuckle; Larry W Robertson; Hans-Joachim Lehmler
Journal:  Environ Toxicol Chem       Date:  2008-02       Impact factor: 3.742

5.  Miniaturised selective pressurised liquid extraction of polychlorinated biphenyls from foodstuffs.

Authors:  J J Ramos; C Dietz; M J González; L Ramos
Journal:  J Chromatogr A       Date:  2006-12-18       Impact factor: 4.759

6.  Comprehensive comparison of classic Soxhlet extraction with Soxtec extraction, ultrasonication extraction, supercritical fluid extraction, microwave assisted extraction and accelerated solvent extraction for the determination of polychlorinated biphenyls in soil.

Authors:  Sune Sporring; Søren Bøwadt; Bo Svensmark; Erland Björklund
Journal:  J Chromatogr A       Date:  2005-10-07       Impact factor: 4.759

7.  On-line clean-up of pressurized liquid extracts for the determination of polychlorinated biphenyls in feedingstuffs and food matrices using gas chromatography-mass spectrometry.

Authors:  A Müller; E Björklund; C von Holst
Journal:  J Chromatogr A       Date:  2001-08-03       Impact factor: 4.759

8.  The effect of dietary glycine on the hepatic tumor promoting activity of polychlorinated biphenyls (PCBs) in rats.

Authors:  Rodica Petruta Bunaciu; Job C Tharappel; Hans-Joachim Lehmler; Izabela Kania-Korwel; Larry W Robertson; Cidambi Srinivasan; Brett T Spear; Howard P Glauert
Journal:  Toxicology       Date:  2007-07-07       Impact factor: 4.221

9.  Metabolism of 2,2',5,5'-tetrachlorobiphenyl: formation of mono- and bis-methyl sulphone metabolites with a selective affinity for the lung and kidney tissues in mice.

Authors:  A Bergman; I Brandt; P O Darnerud; C A Wachtmeister
Journal:  Xenobiotica       Date:  1982-01       Impact factor: 1.908

10.  A reassessment of the nomenclature of polychlorinated biphenyl (PCB) metabolites.

Authors:  Johan Maervoet; Adrian Covaci; Paul Schepens; Courtney D Sandau; Robert J Letcher
Journal:  Environ Health Perspect       Date:  2004-03       Impact factor: 9.031
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  17 in total

1.  Gas chromatographic analysis with chiral cyclodextrin phases reveals the enantioselective formation of hydroxylated polychlorinated biphenyls by rat liver microsomes.

Authors:  Izabela Kania-Korwel; Michael W Duffel; Hans-Joachim Lehmler
Journal:  Environ Sci Technol       Date:  2011-10-19       Impact factor: 9.028

2.  A new player in environmentally induced oxidative stress: polychlorinated biphenyl congener, 3,3'-dichlorobiphenyl (PCB11).

Authors:  Yueming Zhu; Kranti A Mapuskar; Rachel F Marek; Wenjin Xu; Hans-Joachim Lehmler; Larry W Robertson; Keri C Hornbuckle; Douglas R Spitz; Nukhet Aykin-Burns
Journal:  Toxicol Sci       Date:  2013-08-31       Impact factor: 4.849

3.  Atropselective Disposition of 2,2',3,4',6-Pentachlorobiphenyl (PCB 91) and Identification of Its Metabolites in Mice with Liver-Specific Deletion of Cytochrome P450 Reductase.

Authors:  Xianai Wu; Guangshu Zhai; Jerald L Schnoor; Hans-Joachim Lehmler
Journal:  Chem Res Toxicol       Date:  2019-08-26       Impact factor: 3.739

4.  Identification of a sulfate metabolite of PCB 11 in human serum.

Authors:  Fabian A Grimm; Hans-Joachim Lehmler; Wen Xin Koh; Jeanne DeWall; Lynn M Teesch; Keri C Hornbuckle; Peter S Thorne; Larry W Robertson; Michael W Duffel
Journal:  Environ Int       Date:  2016-11-03       Impact factor: 9.621

5.  2,2',3,5',6-Pentachlorobiphenyl (PCB 95) and its hydroxylated metabolites are enantiomerically enriched in female mice.

Authors:  Izabela Kania-Korwel; Christopher D Barnhart; Marianna Stamou; Kim M Truong; Mohammed H M E El-Komy; Pamela J Lein; Peter Veng-Pedersen; Hans-Joachim Lehmler
Journal:  Environ Sci Technol       Date:  2012-09-28       Impact factor: 9.028

Review 6.  Procedures of determining organic trace compounds in municipal sewage sludge-a review.

Authors:  Petra C Lindholm-Lehto; Heidi S J Ahkola; Juha S Knuutinen
Journal:  Environ Sci Pollut Res Int       Date:  2016-12-13       Impact factor: 4.223

7.  Authentication of synthetic environmental contaminants and their (bio)transformation products in toxicology: polychlorinated biphenyls as an example.

Authors:  Xueshu Li; Erika B Holland; Wei Feng; Jing Zheng; Yao Dong; Isaac N Pessah; Michael W Duffel; Larry W Robertson; Hans-Joachim Lehmler
Journal:  Environ Sci Pollut Res Int       Date:  2018-01-10       Impact factor: 4.223

8.  Elimination of inhaled 3,3'-dichlorobiphenyl and the formation of the 4-hydroxylated metabolite.

Authors:  Xin Hu; Hans-Joachim Lehmler; Andrea Adamcakova-Dodd; Peter S Thorne
Journal:  Environ Sci Technol       Date:  2013-04-25       Impact factor: 9.028

9.  Assessment of the disposition of chiral polychlorinated biphenyls in female mdr 1a/b knockout versus wild-type mice using multivariate analyses.

Authors:  Bartłomiej Milanowski; Janina Lulek; Hans-Joachim Lehmler; Izabela Kania-Korwel
Journal:  Environ Int       Date:  2009-11-17       Impact factor: 9.621

10.  Atropselective Partitioning of Polychlorinated Biphenyls in a HepG2 Cell Culture System: Experimental and Modeling Results.

Authors:  Chun-Yun Zhang; Susanne Flor; Gabriele Ludewig; Hans-Joachim Lehmler
Journal:  Environ Sci Technol       Date:  2020-10-15       Impact factor: 9.028
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