Literature DB >> 18975956

"Pure by NMR"?

Timothy D W Claridge1, Stephen G Davies, Mario E C Polywka, Paul M Roberts, Angela J Russell, Edward D Savory, Andrew D Smith.   

Abstract

Integration of a (13)C-(1)H satellite peak of a given (12)C-(1)H parent resonance within a quantitative (1)H NMR spectrum and comparison to the minor component represents a simple protocol for the accurate determination of diastereoisomeric ratios of up to 1000:1 (i.e., 99.8% de).

Year:  2008        PMID： 18975956     DOI： 10.1021/ol802211p

Source DB:  PubMed          Journal:  Org Lett        ISSN： 1523-7052            Impact factor:   6.005


  3 in total

Review 1.  Quantitative 1H NMR. Development and potential of an analytical method: an update.

Authors:  Guido F Pauli; Tanja Gödecke; Birgit U Jaki; David C Lankin
Journal:  J Nat Prod       Date:  2012-04-06       Impact factor: 4.050

2.  NMR quantitation of natural products at the nanomole scale.

Authors:  Doralyn S Dalisay; Tadeusz F Molinski
Journal:  J Nat Prod       Date:  2009-04       Impact factor: 4.050

3.  From arylamine N-acetyltransferase to folate-dependent acetyl CoA hydrolase: impact of folic acid on the activity of (HUMAN)NAT1 and its homologue (MOUSE)NAT2.

Authors:  Nicola Laurieri; Julien Dairou; James E Egleton; Lesley A Stanley; Angela J Russell; Jean-Marie Dupret; Edith Sim; Fernando Rodrigues-Lima
Journal:  PLoS One       Date:  2014-05-13       Impact factor: 3.240
  3 in total

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