| Literature DB >> 18554970 |
Renée Siegel1, Julien Trébosc, Jean-Paul Amoureux, Zhehong Gan.
Abstract
Nitrogen-14 (spin I=1) has always been a nucleus difficult to observe in solid-state NMR and until recently its observation was restricted to one-dimensional (1D) spectra. We present here the first 3D 1H-13C-14N NMR correlation spectrum. This spectrum was acquired on a test sample L-histidine.HCl.H2O using a recently developed technique, which consists in indirectly observing 14N nuclei via dipolar recoupling with an HMQC-type experiment.Entities:
Mesh：
Substances：
Year: 2008 PMID： 18554970 DOI： 10.1016/j.jmr.2008.05.013
Source DB: PubMed Journal: J Magn Reson ISSN： 1090-7807 Impact factor: 2.229