Literature DB >> 18248068

Flow at interfaces: a new device for x-ray surface scattering investigations.

J-F Moulin1, S V Roth, P Müller-Buschbaum.   

Abstract

A fluidic cell based setup is described which allows for microbeam grazing incidence small angle x-ray scattering characterization of the interface between a solid substrate and a flowing liquid. This cell can potentially be used to study in situ a wide variety of systems ranging from synthetic and natural colloids to biological molecules. The selected channel geometry enables the characterization of the solid-liquid interface during mixing of different solutions. As a proof of concept, measurements on an aqueous gold nanoparticle solution in contact with a glass surface are presented that show that the structure at the interface can be probed during flow.

Year:  2008        PMID: 18248068     DOI: 10.1063/1.2816220

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  5 in total

1.  P03, the microfocus and nanofocus X-ray scattering (MiNaXS) beamline of the PETRA III storage ring: the microfocus endstation.

Authors:  Adeline Buffet; André Rothkirch; Ralph Döhrmann; Volker Körstgens; Mottakin M Abul Kashem; Jan Perlich; Gerd Herzog; Matthias Schwartzkopf; Rainer Gehrke; Peter Müller-Buschbaum; Stephan V Roth
Journal:  J Synchrotron Radiat       Date:  2012-05-10       Impact factor: 2.616

Review 2.  Advanced grazing-incidence techniques for modern soft-matter materials analysis.

Authors:  Alexander Hexemer; Peter Müller-Buschbaum
Journal:  IUCrJ       Date:  2015-01-01       Impact factor: 4.769

Review 3.  Functional materials analysis using in situ and in operando X-ray and neutron scattering.

Authors:  Vanessa K Peterson; Christine M Papadakis
Journal:  IUCrJ       Date:  2015-02-03       Impact factor: 4.769

Review 4.  Investigating Polymer-Metal Interfaces by Grazing Incidence Small-Angle X-Ray Scattering from Gradients to Real-Time Studies.

Authors:  Matthias Schwartzkopf; Stephan V Roth
Journal:  Nanomaterials (Basel)       Date:  2016-12-10       Impact factor: 5.076

5.  Development of a sticker sealed microfluidic device for in situ analytical measurements using synchrotron radiation.

Authors:  Itamar T Neckel; Lucas F de Castro; Flavia Callefo; Verônica C Teixeira; Angelo L Gobbi; Maria H Piazzetta; Ricardo A G de Oliveira; Renato S Lima; Rafael A Vicente; Douglas Galante; Helio C N Tolentino
Journal:  Sci Rep       Date:  2021-12-08       Impact factor: 4.379

  5 in total

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