Literature DB >> 18220448

Solvent selection for pressurized liquid extraction of polymeric sorbents used in air sampling.

Toby Primbs1, Susan Genualdi, Staci Massey Simonich.   

Abstract

Pressurized liquid extraction (PLE) was evaluated as a method for extracting semivolatile organic compounds (SOCs) from air sampling media, including quartz fiber filter (QFF), polyurethane foam (PUF), and a polystyrene divinyl benzene copolymer (XAD-2). Hansen solubility parameter plots were used to aid in the PLE solvent selection in order to both reduce coextraction of polyurethane and save time in evaluating solvent compatibility during the initial steps of method development. A PLE solvent composition of 75:25% hexane:acetone was chosen for PUF. The XAD-2 copolymer was not solubilized under the PLE conditions used. The average percent PLE recoveries (and percent relative standard deviations) of 63 SOCs, including polycyclic aromatic hydrocarbons, polychlorinated biphenyls, and organochlorine, amide, triazine, thiocarbamate, and phosphorothioate pesticides, were 76.7 (6.2), 79.3 (8.1), and 93.4 (2.9)% for the QFF, PUF, and XAD-2, respectively.

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Year:  2008        PMID： 18220448      PMCID： PMC4145843          DOI： 10.1897/07-566

Source DB:  PubMed          Journal:  Environ Toxicol Chem        ISSN： 0730-7268            Impact factor:   3.742


  7 in total

1.  Recent extraction techniques for solid matrices-supercritical fluid extraction, pressurized fluid extraction and microwave-assisted extraction: their potential and pitfalls.

Authors:  V Camel
Journal:  Analyst       Date:  2001-07       Impact factor: 4.616

2.  Trace analysis of semivolatile organic compounds in large volume samples of snow, lake water, and groundwater.

Authors:  Sascha Usenko; Kimberly J Hageman; Dave W Schmedding; Glenn R Wilson; Staci L Simonich
Journal:  Environ Sci Technol       Date:  2005-08-15       Impact factor: 9.028

3.  Troubleshooting with cell blanks in PLE extraction.

Authors:  V Fernández-González; G Grueiro-Noche; E Concha-Graña; M I Turnes-Carou; S Muniategui-Lorenzo; P López-Mahía; D Prada-Rodríguez
Journal:  Anal Bioanal Chem       Date:  2005-10-12       Impact factor: 4.142

4.  Development of a pressurized liquid extraction and clean-up procedure for the determination of alpha-endosulfan, beta-endosulfan and endosulfan sulfate in aged contaminated Ethiopian soils.

Authors:  Ahmed Hussen; Rikard Westbom; Negussie Megersa; Lennart Mathiasson; Erland Björklund
Journal:  J Chromatogr A       Date:  2005-12-20       Impact factor: 4.759

5.  Comparison of pressurized fluid extraction, Soxhlet extraction and sonication for the determination of polycyclic aromatic hydrocarbons in urban air and diesel exhaust particulate matter.

Authors:  M Rynö; L Rantanen; E Papaioannou; A G Konstandopoulos; T Koskentalo; K Savela
Journal:  J Environ Monit       Date:  2006-03-09

6.  Global distribution of persistent organochlorine compounds.

Authors:  S L Simonich; R A Hites
Journal:  Science       Date:  1995-09-29       Impact factor: 47.728

7.  Atmospheric outflow of anthropogenic semivolatile organic compounds from East Asia in spring 2004.

Authors:  Toby Primbs; Staci Simonich; David Schmedding; Glenn Wilson; Dan Jaffe; Akinori Takami; Shungo Kato; Shiro Hatakeyama; Yoshizumi Kajii
Journal:  Environ Sci Technol       Date:  2007-05-15       Impact factor: 9.028
  7 in total
  9 in total

1.  Concentration and photochemistry of PAHs, NPAHs, and OPAHs and toxicity of PM2.5 during the Beijing Olympic Games.

Authors:  Wentao Wang; Narumol Jariyasopit; Jill Schrlau; Yuling Jia; Shu Tao; Tian-Wei Yu; Roderick H Dashwood; Wei Zhang; Xuejun Wang; Staci L Massey Simonich
Journal:  Environ Sci Technol       Date:  2011-07-18       Impact factor: 9.028

2.  Comparison of lichen, conifer needles, passive air sampling devices, and snowpack as passive sampling media to measure semi-volatile organic compounds in remote atmospheres.

Authors:  Jill E Schrlau; Linda Geiser; Kimberly J Hageman; Dixon H Landers; Staci Massey Simonich
Journal:  Environ Sci Technol       Date:  2011-11-16       Impact factor: 9.028

3.  PAH intermediates: Links between the atmosphere and biological systems.

Authors:  Staci L Massey Simonich; Oleksii Motorykin; Narumol Jariyasopit
Journal:  Chem Biol Interact       Date:  2010-09-16       Impact factor: 5.192

4.  Improved separation of complex polycyclic aromatic hydrocarbon mixtures using novel column combinations in GC × GC/ToF-MS.

Authors:  Carlos Manzano; Eunha Hoh; Staci L Massey Simonich
Journal:  Environ Sci Technol       Date:  2012-07-06       Impact factor: 9.028

5.  Inhalation cancer risk associated with exposure to complex polycyclic aromatic hydrocarbon mixtures in an electronic waste and urban area in South China.

Authors:  Jing Wang; Shejun Chen; Mi Tian; Xiaobo Zheng; Leah Gonzales; Takeshi Ohura; Bixian Mai; Staci L Massey Simonich
Journal:  Environ Sci Technol       Date:  2012-08-22       Impact factor: 9.028

6.  Trans-Pacific and regional atmospheric transport of polycyclic aromatic hydrocarbons and pesticides in biomass burning emissions to western North America.

Authors:  Susan A Genualdi; Robert K Killin; Jim Woods; Glenn Wilson; David Schmedding; Staci L Massey Simonich
Journal:  Environ Sci Technol       Date:  2009-02-15       Impact factor: 9.028

7.  Enantiomeric signatures of organochlorine pesticides in Asian, trans-Pacific, and western U.S. air masses.

Authors:  Susan A Genualdi; Staci L Massey Simonich; Toby K Primbs; Terry F Bidleman; Liisa M Jantunen; Keon-Sang Ryoo; Tong Zhu
Journal:  Environ Sci Technol       Date:  2009-04-15       Impact factor: 9.028

8.  Quantification of complex polycyclic aromatic hydrocarbon mixtures in standard reference materials using comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry.

Authors:  Carlos Manzano; Eunha Hoh; Staci L Massey Simonich
Journal:  J Chromatogr A       Date:  2013-07-30       Impact factor: 4.759

9.  Estimated reduction in cancer risk due to PAH exposures if source control measures during the 2008 Beijing Olympics were sustained.

Authors:  Yuling Jia; Dave Stone; Wentao Wang; Jill Schrlau; Shu Tao; Staci L Massey Simonich
Journal:  Environ Health Perspect       Date:  2011-06       Impact factor: 9.031
  9 in total

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