Literature DB >> 18163715

KMC-1: a high resolution and high flux soft x-ray beamline at BESSY.

F Schaefers1, M Mertin, M Gorgoi.   

Abstract

The crystal monochromator beamline KMC-1 at a BESSY II bending magnet covers the energy range from soft (1.7 keV) to hard x-rays (12 keV) employing the (n,-n) double crystal arrangement with constant beam offset. The monochromator is equipped with three sets of crystals, InSb, Si (111), and Si (422) which are exchangeable in situ within a few minutes. Beamline and monochromator have been optimized for high flux and high resolution. This could be achieved by (1) a windowless setup under ultrahigh-vacuum conditions up to the experiment, (2) by the use of only three optical elements to minimize reflection losses, (3) by collecting an unusually large horizontal radiation fan (6 mrad) with the toroidal premirror, and (4) the optimization of the crystal optics to the soft x-ray range necessitating quasibackscattering crystal geometry (theta(Bragg,max)=82 degrees) delivering crystal limited resolution. The multipurpose beamline is in use for a variety of user facilities such as extended x-ray absorption fine structure, ((Bio-)EXAFS) near-edge x-ray absorption fine structure (NEXAFS), absorption and fluorescence spectroscopy. Due to the windowless UHV setup the k edges of the technologically and biologically important elements such as Si, P, and S are accessible. In addition to these experiments this beamline is now extensively used for photoelectron spectroscopy at high kinetic energies. Photon flux in the 10(11)-10(12) photons/s range and beamline resolving powers of more than E/DeltaE approximately 100.000 have been measured at selected energies employing Si (nnn) high order radiation in quasibackscattering geometry, thus photoelectron spectroscopy with a total instrumental resolution of about 150 meV is possible. This article describes the design features of the beamline and reports some experimental results in the above mentioned fields.

Entities:  

Year:  2007        PMID: 18163715     DOI: 10.1063/1.2808334

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  7 in total

1.  Soft x-ray reflectometry, hard x-ray photoelectron spectroscopy and transmission electron microscopy investigations of the internal structure of TiO2(Ti)/SiO2/Si stacks.

Authors:  Elena O Filatova; Igor V Kozhevnikov; Andrey A Sokolov; Evgeniy V Ubyivovk; Sergey Yulin; Mihaela Gorgoi; Franz Schäfers
Journal:  Sci Technol Adv Mater       Date:  2012-02-02       Impact factor: 8.090

2.  Facilities for macromolecular crystallography at the Helmholtz-Zentrum Berlin.

Authors:  Uwe Mueller; Nora Darowski; Martin R Fuchs; Ronald Förster; Michael Hellmig; Karthik S Paithankar; Sandra Pühringer; Michael Steffien; Georg Zocher; Manfred S Weiss
Journal:  J Synchrotron Radiat       Date:  2012-03-20       Impact factor: 2.616

3.  Insights into the Mechanism of a Covalently Linked Organic Dye-Cobaloxime Catalyst System for Dye-Sensitized Solar Fuel Devices.

Authors:  Palas Baran Pati; Lei Zhang; Bertrand Philippe; Ricardo Fernández-Terán; Sareh Ahmadi; Lei Tian; Håkan Rensmo; Leif Hammarström; Haining Tian
Journal:  ChemSusChem       Date:  2017-05-03       Impact factor: 8.928

4.  Identifying the nature of surface chemical modification for directed self-assembly of block copolymers.

Authors:  Laura Evangelio; Federico Gramazio; Matteo Lorenzoni; Michaela Gorgoi; Francisco Miguel Espinosa; Ricardo García; Francesc Pérez-Murano; Jordi Fraxedas
Journal:  Beilstein J Nanotechnol       Date:  2017-09-21       Impact factor: 3.649

5.  Impact of SnF2 Addition on the Chemical and Electronic Surface Structure of CsSnBr3.

Authors:  Claudia Hartmann; Satyajit Gupta; Tatyana Bendikov; Xeniya Kozina; Thomas Kunze; Roberto Félix; Gary Hodes; Regan G Wilks; David Cahen; Marcus Bär
Journal:  ACS Appl Mater Interfaces       Date:  2020-03-02       Impact factor: 9.229

6.  Interface Engineering to Create a Strong Spin Filter Contact to Silicon.

Authors:  C Caspers; A Gloskovskii; M Gorgoi; C Besson; M Luysberg; K Z Rushchanskii; M Ležaić; C S Fadley; W Drube; M Müller
Journal:  Sci Rep       Date:  2016-03-15       Impact factor: 4.379

7.  Re-distribution of oxygen at the interface between γ-Al2O3 and TiN.

Authors:  E O Filatova; A S Konashuk; S S Sakhonenkov; A A Sokolov; V V Afanas'ev
Journal:  Sci Rep       Date:  2017-07-03       Impact factor: 4.379

  7 in total

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