Literature DB >> 18007399

Synthesis and characterization of dimethacrylate monomer with high molecular weight for root canal filling materials.

Fang Liu1, Jing-wie He, Zheng-mei Lin, Jun-qi Ling, De-min Jia.   

Abstract

A new dimethacrylate monomer 9,9'-bis[4-(2'-hydroxy-3'-methacryloyloxy-propoxy)phenyl] fluorene (3) with a molecular weight of 634 was synthesized in 51.4% yield by addition of a glycidyl ether group to 9,9'-bis(4-hydroxyphenyl) fluorene (1) by the reaction of compound 1 with epichlorohydrin, and then introducing the methacrylate moiety by the reaction of the epoxy group with methacrylic acid. The structure of monomer 3 was confirmed by FT-IR, (1)H-NMR, mass spectra and elemental analysis.

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Year:  2006        PMID: 18007399      PMCID: PMC6148667          DOI: 10.3390/11120953

Source DB:  PubMed          Journal:  Molecules        ISSN: 1420-3049            Impact factor:   4.411


  9 in total

1.  A comparative evaluation of sealing ability of rootcanal sealers.

Authors:  B S Suprabha; P Sudha; M Vidya
Journal:  Indian J Dent Res       Date:  2002 Jan-Mar

2.  A comparison of three different methods for the quantification of the in vitro wear of dental materials.

Authors:  S D Heintze; A Cavalleri; M Forjanic; G Zellweger; V Rousson
Journal:  Dent Mater       Date:  2005-12-28       Impact factor: 5.304

3.  A comparative study of physicochemical properties of AH Plus and Epiphany root canal sealants.

Authors:  M A Versiani; J R Carvalho-Junior; M I A F Padilha; S Lacey; E A Pascon; M D Sousa-Neto
Journal:  Int Endod J       Date:  2006-06       Impact factor: 5.264

4.  Development of a new photocurable composite resin with reduced curing shrinkage.

Authors:  C-M Chung; J-G Kim; M-S Kim; K-M Kim; K-N Kim
Journal:  Dent Mater       Date:  2002-03       Impact factor: 5.304

5.  Synthesis and photopolymerization of low shrinkage methacrylate monomers containing bulky substituent groups.

Authors:  Junhao Ge; Marianela Trujillo; Jeffrey Stansbury
Journal:  Dent Mater       Date:  2005-06-29       Impact factor: 5.304

6.  Synthesis and photopolymerization of trifunctional methacrylates and their application as dental monomers.

Authors:  Chan-Moon Chung; Min-Sung Kim; Joong-Gon Kim; Doo-Ok Jang
Journal:  J Biomed Mater Res       Date:  2002-12-15

7.  An evaluation of microbial leakage in roots filled with a thermoplastic synthetic polymer-based root canal filling material (Resilon).

Authors:  Guy Shipper; Dag Ørstavik; Fabricio Batista Teixeira; Martin Trope
Journal:  J Endod       Date:  2004-05       Impact factor: 4.171

8.  Polymerization contraction and conversion of light-curing BisGMA-based methacrylate resins.

Authors:  B A Venhoven; A J de Gee; C L Davidson
Journal:  Biomaterials       Date:  1993-09       Impact factor: 12.479

9.  Synthesis, characterization and evaluation of urethane derivatives of Bis-GMA.

Authors:  Chetan A Khatri; Jeffery W Stansbury; Carl R Schultheisz; Joseph M Antonucci
Journal:  Dent Mater       Date:  2003-11       Impact factor: 5.304

  9 in total
  1 in total

1.  Synthesis of a novel tertiary amine containing urethane dimethacrylate monomer (UDMTA) and its application in dental resin.

Authors:  Dongliang Liu; Fang Liu; Jingwei He; Lippo V J Lassila; Pekka K Vallittu
Journal:  J Mater Sci Mater Med       Date:  2013-03-02       Impact factor: 3.896

  1 in total

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