Literature DB >> 17873845

Structure elucidation of a pyrazolo[3,4]pyran derivative by NMR spectroscopy.

Xuehui Liu1, Yuxin Cui.   

Abstract

The structure of a representative pyrazolo[3,4]pyran derivative was determined by 1D and 2D NMR techniques. Complete 1H and 13C chemical shifts for this compound are reported. Careful analysis of the HMBC (Heteronuclear Multi-Bond Correlation) spectrum helped to elucidate the configuration of the derivative around C7 and C8. The results showed that the characteristic double-strong and double-weak cross peak pattern in the HMBC spectrum for C7 and C8 might be useful for establishing the structures of other pyrazolo[3,4]pyran derivatives.

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Year:  2007        PMID: 17873845      PMCID: PMC6149502          DOI: 10.3390/12051117

Source DB:  PubMed          Journal:  Molecules        ISSN: 1420-3049            Impact factor:   4.411


  5 in total

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  5 in total

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