Literature DB >> 17566331

Determination of anti-inflammatory drugs and estrogens in water by HPLC with UV detection.

Anna Stafiej1, Krystyna Pyrzynska, Fiona Regan.   

Abstract

An analytical method based on LC and UV detection has been developed for the determination of anti-inflammatory compounds and estrogens in water samples. The drugs investigated were diclofenac, ketoprofen, ibuprofen, naproxen, clofibric acid, estriol, 17beta-estradiol, estrone and ethynylestradiol. The detection limits were in the range of 6-74 microg/L and 0.041 -0.16 mg/L for acidic pharmaceuticals and estrogens, respectively, using narrow-bore C18 analytical column. Analyte enrichment from water samples was achieved by SPE procedure using polymeric Strata-X cartridges. Average recoveries obtained from 2.5 L of surface water sample were in the range of 77-98%.

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Year:  2007        PMID: 17566331     DOI: 10.1002/jssc.200600433

Source DB:  PubMed          Journal:  J Sep Sci        ISSN: 1615-9306            Impact factor:   3.645


  4 in total

1.  Graphitic carbon nitride and APTES modified advanced electrochemical biosensor for detection of 17β-estradiol in spiked food samples.

Authors:  M S Bacchu; M R Ali; M N Hasan; M R A Mamun; M I Hossain; M Z H Khan
Journal:  RSC Adv       Date:  2022-06-06       Impact factor: 4.036

2.  Electrochemical biosensor for detection of 17β-estradiol using semi-conducting polymer and horseradish peroxidase.

Authors:  Kamila Spychalska; Dorota Zając; Joanna Cabaj
Journal:  RSC Adv       Date:  2020-03-03       Impact factor: 4.036

3.  Ultra high performance liquid chromatography tandem mass spectrometry for rapid analysis of trace organic contaminants in water.

Authors:  Tarun Anumol; Sylvain Merel; Bradley O Clarke; Shane A Snyder
Journal:  Chem Cent J       Date:  2013-06-18       Impact factor: 4.215

4.  Development of Simultaneous Derivative Spectrophotometric and HPLC Methods for Determination of 17-Beta-Estradiol and Drospirenone in Combined Dosage Form.

Authors:  Zeynep Aydoğmuş; Ece Merve Yılmaz; Sevgi Yörüsün; Samet Akpınar
Journal:  Int Sch Res Notices       Date:  2015-04-27
  4 in total

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