Literature DB >> 17389984

Synthesis of para-methoxybenzyl (PMB) ethers under neutral conditions.

Ernest O Nwoye1, Gregory B Dudley.   

Abstract

2-(4-Methoxybenzyloxy)-4-methylquinoline reacts with methyl triflate in the presence of alcohols to generate a neutral organic salt that transfers the para-methoxybenzyl (PMB) protecting group onto alcohols in high yield and under mild conditions.

Entities:  

Year:  2007        PMID： 17389984     DOI： 10.1039/b617926f

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  5 in total

1.  Formation of DPM ethers using O-diphenylmethyl trichloroacetimidate under thermal conditions.

Authors:  Kyle T Howard; Brian C Duffy; Matthew R Linaburg; John D Chisholm
Journal:  Org Biomol Chem       Date:  2016-02-07       Impact factor: 3.876

2.  Convergent route to the spirohexenolide macrocycle.

Authors:  Brian D Jones; James J La Clair; Curtis E Moore; Arnold L Rheingold; Michael D Burkart
Journal:  Org Lett       Date:  2010-10-15       Impact factor: 6.005

3.  A 16-step synthesis of the isoryanodane diterpene (+)-perseanol.

Authors:  Arthur Han; Yujia Tao; Sarah E Reisman
Journal:  Nature       Date:  2019-09-25       Impact factor: 49.962

4.  Total Synthesis of Mycinolide IV and Path-Scouting for Aldgamycin N.

Authors:  Bart Herlé; Georg Späth; Lucas Schreyer; Alois Fürstner
Journal:  Angew Chem Int Ed Engl       Date:  2021-02-26       Impact factor: 15.336

5.  Convenient method for preparing benzyl ethers and esters using 2-benzyloxypyridine.

Authors:  Susana S Lopez; Gregory B Dudley
Journal:  Beilstein J Org Chem       Date:  2008-11-26       Impact factor: 2.883
  5 in total

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