Literature DB >> 17268642

Practical synthesis of chiral 9,9'-spirobixanthene-1,1'-diol.

Weicheng Zhang1, Shulin Wu, Zhaoguo Zhang, Hemant Yennawar, Xumu Zhang.   

Abstract

A concise four-step synthesis of 9,9'-spirobixanthene-1,1'-diol is reported, featuring a practical preparation at large scale without the use of column chromatography purification. Co-crystallization with N-benzylcinchonidinium chloride and N-benzylquininium chloride rendered the optically pure product in both enantiomers.

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Year:  2006        PMID: 17268642     DOI: 10.1039/b610879b

Source DB:  PubMed          Journal:  Org Biomol Chem        ISSN: 1477-0520            Impact factor:   3.876


  1 in total

1.  Crystal structures of anhydrous and hydrated N-benzyl-cinchonidinium bromide.

Authors:  Daron E Janzen; Maya S Butler; Eric W Reinheimer
Journal:  Acta Crystallogr E Crystallogr Commun       Date:  2022-05-17
  1 in total

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