Literature DB >> 17211083

Application of a hybrid pixel detector to powder diffraction.

S Basolo1, J F Bérar, N Boudet, P Breugnon, B Caillot, J C Clemens, P Delpierre, B Dinkespiler, S Hustache, I Koudobine, Ch Meessen, M Menouni, C Mouget, H Palancher, P Pangaud, R Potheau, E Vigeolas.   

Abstract

Results obtained using a hybrid pixel photon-counting detector in powder diffraction experiments are presented. The detector works at room temperature and its dynamic response ranges from 0.01 photons pixel(-1) s(-1) up to 10(6) photons pixel(-1) s(-1). The pixel sizes are 0.33 mm x 0.33 mm for a total area of 68 mm x 68 mm. On recording high-resolution diffraction patterns of powders, a reduction of the experimental time by more than a factor of 20 is obtained without loss of data quality. The example of an X-zeolite shows that such detectors can be used for very demanding anomalous experiments. In situ experiments of quenching liquid oxides show that frames of 0.01 s can be achieved for studying such processes.

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Year:  2006        PMID: 17211083     DOI: 10.1107/S0909049506048783

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  2 in total

1.  Full reciprocal-space mapping up to 2000 K under controlled atmosphere: the multipurpose QMAX furnace.

Authors:  René Guinebretière; Stephan Arnaud; Nils Blanc; Nathalie Boudet; Elsa Thune; David Babonneau; Olivier Castelnau
Journal:  J Appl Crystallogr       Date:  2020-04-23       Impact factor: 3.304

2.  The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source.

Authors:  Anna Bergamaschi; Antonio Cervellino; Roberto Dinapoli; Fabia Gozzo; Beat Henrich; Ian Johnson; Philipp Kraft; Aldo Mozzanica; Bernd Schmitt; Xintian Shi
Journal:  J Synchrotron Radiat       Date:  2010-07-22       Impact factor: 2.616

  2 in total

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