| Literature DB >> 17211083 |
S Basolo1, J F Bérar, N Boudet, P Breugnon, B Caillot, J C Clemens, P Delpierre, B Dinkespiler, S Hustache, I Koudobine, Ch Meessen, M Menouni, C Mouget, H Palancher, P Pangaud, R Potheau, E Vigeolas.
Abstract
Results obtained using a hybrid pixel photon-counting detector in powder diffraction experiments are presented. The detector works at room temperature and its dynamic response ranges from 0.01 photons pixel(-1) s(-1) up to 10(6) photons pixel(-1) s(-1). The pixel sizes are 0.33 mm x 0.33 mm for a total area of 68 mm x 68 mm. On recording high-resolution diffraction patterns of powders, a reduction of the experimental time by more than a factor of 20 is obtained without loss of data quality. The example of an X-zeolite shows that such detectors can be used for very demanding anomalous experiments. In situ experiments of quenching liquid oxides show that frames of 0.01 s can be achieved for studying such processes.Entities:
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Year: 2006 PMID: 17211083 DOI: 10.1107/S0909049506048783
Source DB: PubMed Journal: J Synchrotron Radiat ISSN: 0909-0495 Impact factor: 2.616