Literature DB >> 17168615

Synthesis of oligo(ethylene glycol) toward 44-mer.

Saleh A Ahmed1, Mutsuo Tanaka.   

Abstract

A synthetic method for oligo(ethylene glycol) toward 44-mer (FW = 1956.35) is described. Reiteration of Williamson's ether synthesis and hydrogenation to remove protecting benzyl group affords desired oligo(ethylene glycol) toward 44-mer in moderate yields. The advantages in this method are use of commercially easily available materials as starting materials and procedures avoiding difficulty in purification of the products as much as possible.

Entities:  

Mesh:

Substances:

Year:  2006        PMID: 17168615     DOI: 10.1021/jo0617464

Source DB:  PubMed          Journal:  J Org Chem        ISSN: 0022-3263            Impact factor:   4.354


  5 in total

1.  Solid Phase Stepwise Synthesis of Polyethylene Glycols.

Authors:  Ashok Khanal; Shiyue Fang
Journal:  Chemistry       Date:  2017-10-06       Impact factor: 5.236

2.  Efficient synthesis of diverse heterobifunctionalized clickable oligo(ethylene glycol) linkers: potential applications in bioconjugation and targeted drug delivery.

Authors:  Lalit N Goswami; Zachary H Houston; Saurav J Sarma; Satish S Jalisatgi; M Frederick Hawthorne
Journal:  Org Biomol Chem       Date:  2013-02-21       Impact factor: 3.876

3.  Soft Nanotubes Derivatized with Short PEG Chains for Thermally Controllable Extraction and Separation of Peptides.

Authors:  Naohiro Kameta; Wuxiao Ding; Jiuchao Dong
Journal:  ACS Omega       Date:  2017-09-26

4.  Stepwise PEG synthesis featuring deprotection and coupling in one pot.

Authors:  Dhananjani N A M Eriyagama; Yipeng Yin; Logan Mikesell; Bao-Yuan Lu; Shiyue Fang
Journal:  Beilstein J Org Chem       Date:  2021-12-28       Impact factor: 2.883

5.  Mapping the binding site topology of amyloid protein aggregates using multivalent ligands.

Authors:  Elena Sanna; Margarida Rodrigues; Steven G Fagan; Timothy S Chisholm; Klara Kulenkampff; David Klenerman; Maria Grazia Spillantini; Franklin I Aigbirhio; Christopher A Hunter
Journal:  Chem Sci       Date:  2021-06-07       Impact factor: 9.825

  5 in total

北京卡尤迪生物科技股份有限公司 © 2022-2023.