Literature DB >> 17088090

Improved resolution in (13)C solid-state spectra through spin-state-selection.

René Verel1, Theofanis Manolikas, Ansgar B Siemer, Beat H Meier.   

Abstract

The application of a spin-state-selective coherence transfer experiment (INADEQUATE-SSS) to solid-state NMR spectroscopy is described. Two-dimensional (13)C double-quantum/single-quantum spectra without J splittings in both dimensions lead to enhanced spectral resolution. The method is demonstrated to significantly improve the spectral resolution of the crowded C'-C(alpha) region of two proteins.

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Year:  2006        PMID： 17088090     DOI： 10.1016/j.jmr.2006.09.024

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


  2 in total

1.  New insights into the structure and reduction of graphite oxide.

Authors:  Wei Gao; Lawrence B Alemany; Lijie Ci; Pulickel M Ajayan
Journal:  Nat Chem       Date:  2009-07-05       Impact factor: 24.427

2.  Long-observation-window band-selective homonuclear decoupling: increased sensitivity and resolution in solid-state NMR spectroscopy of proteins.

Authors:  Jochem O Struppe; Chen Yang; Yachong Wang; Roy V Hernandez; Lisa M Shamansky; Leonard J Mueller
Journal:  J Magn Reson       Date:  2013-09-13       Impact factor: 2.229
  2 in total

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