Literature DB >> 17048845

Simplification of the Mitsunobu reaction. Di-p-chlorobenzyl azodicarboxylate: a new azodicarboxylate.

Bruce H Lipshutz1, David W Chung, Brian Rich, Ricardo Corral.   

Abstract

Di-p-chlorobenzyl azodicarboxylate (DCAD) is introduced as a novel, stable, solid alternative to DEAD and DIAD for a variety of Mitsunobu couplings. DCAD/Ph(3)P-mediated reactions in CH(2)Cl(2) generate a readily separable hydrazine byproduct. [reaction: see text]

Entities:  

Year:  2006        PMID： 17048845     DOI： 10.1021/ol0618757

Source DB:  PubMed          Journal:  Org Lett        ISSN： 1523-7052            Impact factor:   6.005


  9 in total

1.  An Overview of Stereoselective Synthesis of α-Aminophosphonic Acids and Derivatives.

Authors:  Mario Ordóñez; Haydée Rojas-Cabrera; Carlos Cativiela
Journal:  Tetrahedron       Date:  2009-01-03       Impact factor: 2.457

2.  Recent Progress on the Stereoselective Synthesis of Cyclic Quaternary alpha-Amino Acids.

Authors:  Carlos Cativiela; Mario Ordóñez
Journal:  Tetrahedron Asymmetry       Date:  2009-01-30

3.  Practical catalytic asymmetric synthesis of diaryl-, aryl heteroaryl-, and diheteroarylmethanols.

Authors:  Luca Salvi; Jeung Gon Kim; Patrick J Walsh
Journal:  J Am Chem Soc       Date:  2009-09-02       Impact factor: 15.419

4.  Synthesis of N,N-Diethylbenzamides via a Non-Classical Mitsunobu Reaction.

Authors:  J Mason Hoffman; Justin N Miller; Margaret E Gardner; Danielle R LePar; Rongson Pongdee
Journal:  Synth Commun       Date:  2014-01-01       Impact factor: 2.007

5.  A biomimetic strategy to access the silybins: total synthesis of (-)-isosilybin A.

Authors:  Benjamin R McDonald; Antoinette E Nibbs; Karl A Scheidt
Journal:  Org Lett       Date:  2014-12-17       Impact factor: 6.005

6.  Oxidative coupling of sp 2 and sp 3 carbon-hydrogen bonds to construct dihydrobenzofurans.

Authors:  Jiang-Ling Shi; Ding Wang; Xi-Sha Zhang; Xiao-Lei Li; Yu-Qin Chen; Yu-Xue Li; Zhang-Jie Shi
Journal:  Nat Commun       Date:  2017-08-10       Impact factor: 14.919

7.  A novel and highly efficient esterification process using triphenylphosphine oxide with oxalyl chloride.

Authors:  Mingzhu Jia; Lixue Jiang; Fanfan Niu; Yu Zhang; Xiaoling Sun
Journal:  R Soc Open Sci       Date:  2018-02-21       Impact factor: 2.963

8.  A Facile Synthetic Method for Anhydride from Carboxylic Acid with the Promotion of Triphenylphosphine Oxide and Oxaloyl Chloride.

Authors:  Mengyu Lu; Huihui Fan; Qing Liu; Xiaoling Sun
Journal:  ACS Omega       Date:  2022-09-13

9.  N-1 regioselective Michael-type addition of 5-substituted uracils to (2-hydroxyethyl) acrylate.

Authors:  Sławomir Boncel; Dominika Osyda; Krzysztof Z Walczak
Journal:  Beilstein J Org Chem       Date:  2007-11-08       Impact factor: 2.883
  9 in total

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