Literature DB >> 17027306

A field-sweep/field-lock system for superconducting magnets--Application to high-field EPR.

Thorsten Maly1, Jeff Bryant, David Ruben, Robert G Griffin.   

Abstract

We describe a field-lock/field-sweep system for the use in superconducting magnets. The system is based on a commercially available field mapping unit and a custom designed broad-band 1H NMR probe. The NMR signal of a small water sample is used in a feedback loop to set and control the magnetic field to high accuracy. The current instrumental configuration allows field sweeps of +/-0.4 T and a resolution of up to 10(-5) T (0.1 G) and the performance of the system is demonstrated in a high-field electron paramagnetic resonance (EPR) application. The system should also be of utility in other experiments requiring precise and reproducible sweeps of the magnetic field such as DNP, ENDOR or PELDOR.

Entities:  

Mesh:

Year:  2006        PMID: 17027306      PMCID: PMC2518535          DOI: 10.1016/j.jmr.2006.09.012

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  5 in total

1.  A continuous-wave and pulsed electron spin resonance spectrometer operating at 275 GHz.

Authors:  H Blok; J A J M Disselhorst; S B Orlinskii; J Schmidt
Journal:  J Magn Reson       Date:  2004-01       Impact factor: 2.229

2.  High-frequency ESR at ACERT.

Authors:  Keith A Earle; Boris Dzikovski; Wulf Hofbauer; Jozef K Moscicki; Jack H Freed
Journal:  Magn Reson Chem       Date:  2005-11       Impact factor: 2.447

3.  Electron-nuclear cross polarization.

Authors:  V Weis; R G Griffin
Journal:  Solid State Nucl Magn Reson       Date:  2005-11-18       Impact factor: 2.293

4.  Pulsed electron-nuclear double resonance (ENDOR) at 140 GHz.

Authors:  M Bennati; C T Farrar; J A Bryant; S J Inati; V Weis; G J Gerfen; P Riggs-Gelasco; J Stubbe; R G Griffin
Journal:  J Magn Reson       Date:  1999-06       Impact factor: 2.229

5.  Pulsed 180-GHz EPR/ENDOR/PELDOR spectroscopy.

Authors:  M M Hertel; V P Denysenkov; M Bennati; T F Prisner
Journal:  Magn Reson Chem       Date:  2005-11       Impact factor: 2.447

  5 in total
  13 in total

1.  2H-DNP-enhanced 2H-13C solid-state NMR correlation spectroscopy.

Authors:  Thorsten Maly; Loren B Andreas; Albert A Smith; Robert G Griffin
Journal:  Phys Chem Chem Phys       Date:  2010-05-11       Impact factor: 3.676

2.  Rigid orthogonal bis-TEMPO biradicals with improved solubility for dynamic nuclear polarization.

Authors:  Eric L Dane; Björn Corzilius; Egon Rizzato; Pierre Stocker; Thorsten Maly; Albert A Smith; Robert G Griffin; Olivier Ouari; Paul Tordo; Timothy M Swager
Journal:  J Org Chem       Date:  2012-02-06       Impact factor: 4.354

Review 3.  Dynamic nuclear polarization at high magnetic fields.

Authors:  Thorsten Maly; Galia T Debelouchina; Vikram S Bajaj; Kan-Nian Hu; Chan-Gyu Joo; Melody L Mak-Jurkauskas; Jagadishwar R Sirigiri; Patrick C A van der Wel; Judith Herzfeld; Richard J Temkin; Robert G Griffin
Journal:  J Chem Phys       Date:  2008-02-07       Impact factor: 3.488

4.  1H dynamic nuclear polarization based on an endogenous radical.

Authors:  Thorsten Maly; Dongtao Cui; Robert G Griffin; Anne-Frances Miller
Journal:  J Phys Chem B       Date:  2012-06-07       Impact factor: 2.991

5.  A 140 GHz pulsed EPR/212 MHz NMR spectrometer for DNP studies.

Authors:  Albert A Smith; Björn Corzilius; Jeffrey A Bryant; Ronald DeRocher; Paul P Woskov; Richard J Temkin; Robert G Griffin
Journal:  J Magn Reson       Date:  2012-07-20       Impact factor: 2.229

6.  Quantum mechanical theory of dynamic nuclear polarization in solid dielectrics.

Authors:  Kan-Nian Hu; Galia T Debelouchina; Albert A Smith; Robert G Griffin
Journal:  J Chem Phys       Date:  2011-03-28       Impact factor: 3.488

7.  Off-resonance NOVEL.

Authors:  Sheetal K Jain; Guinevere Mathies; Robert G Griffin
Journal:  J Chem Phys       Date:  2017-10-28       Impact factor: 3.488

8.  Overhauser dynamic nuclear polarization (ODNP)-enhanced two-dimensional proton NMR spectroscopy at low magnetic fields.

Authors:  Timothy J Keller; Thorsten Maly
Journal:  Magn Reson (Gott)       Date:  2021-04-12

9.  Dynamic nuclear polarization with a rigid biradical.

Authors:  Yoh Matsuki; Thorsten Maly; Olivier Ouari; Hakim Karoui; François Le Moigne; Egon Rizzato; Sevdalina Lyubenova; Judith Herzfeld; Thomas Prisner; Paul Tordo; Robert G Griffin
Journal:  Angew Chem Int Ed Engl       Date:  2009       Impact factor: 15.336

10.  In situ high-field dynamic nuclear polarization--direct and indirect polarization of 13C nuclei.

Authors:  Thorsten Maly; Anne-Frances Miller; Robert G Griffin
Journal:  Chemphyschem       Date:  2010-04-06       Impact factor: 3.102

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