Literature DB >> 16495620

Multilayer X-ray optics at CHESS.

Alexander Kazimirov1, Detlef M Smilgies, Qun Shen, Xianghui Xiao, Quan Hao, Ernest Fontes, Donald H Bilderback, Sol M Gruner, Yuriy Platonov, Vladimir V Martynov.   

Abstract

Almost half of the X-ray beamlines at the Cornell High Energy Synchrotron Source (CHESS) are based on multilayer optics. ;Traditional' multilayers with an energy resolution of DeltaE/E approximately 2% are routinely used to deliver X-ray flux enhanced by a factor of 10(2) in comparison with standard Si(111) optics. Sagittal-focusing multilayers with fixed radius provide an additional factor of 10 gain in flux density. High-resolution multilayer optics with DeltaE/E approximately 0.2% are now routinely used by MacCHESS crystallographers. New wide-bandpass multilayers with DeltaE/E = 5% and 10% have been designed and tested for potential applications in macromolecular crystallography. Small d-spacing multilayers with d < or = 20 A have been successfully used to extend the energy range of multilayer optics. Analysis of the main characteristics of the Mo/B4C and W/B4C small d-spacing multilayer optics shows enhancement in their performance at higher energies. Chemical vapour deposited SiC, with a bulk thermal conductivity of a factor of two higher than that of silicon, has been successfully introduced as a substrate material for multilayer optics. Characteristics of different types of multilayer optics at CHESS beamlines and their applications in a variety of scattering, diffraction and imaging techniques are discussed.

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Year:  2006        PMID: 16495620     DOI: 10.1107/S0909049506002846

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  8 in total

1.  Time-resolved synchrotron diffraction and theoretical studies of very short-lived photo-induced molecular species.

Authors:  Philip Coppens; Jason Benedict; Marc Messerschmidt; Irina Novozhilova; Tim Graber; Yu-Sheng Chen; Ivan Vorontsov; Stephan Scheins; Shao-Liang Zheng
Journal:  Acta Crystallogr A       Date:  2010-02-18       Impact factor: 2.290

2.  Feasibility of one-shot-per-crystal structure determination using Laue diffraction.

Authors:  Sterling Cornaby; Doletha M E Szebenyi; Detlef-M Smilgies; David J Schuller; Richard Gillilan; Quan Hao; Donald H Bilderback
Journal:  Acta Crystallogr D Biol Crystallogr       Date:  2009-12-21

3.  Scherrer grain-size analysis adapted to grazing-incidence scattering with area detectors.

Authors:  Detlef-M Smilgies
Journal:  J Appl Crystallogr       Date:  2009-10-15       Impact factor: 3.304

4.  Nanocomposite characterization on multiple length scales using µSAXS.

Authors:  Ruipeng Li; Sterling Cornaby; Marleen Kamperman; Detlef-M Smilgies
Journal:  J Synchrotron Radiat       Date:  2011-07-08       Impact factor: 2.616

5.  Study of interface reaction in a B4C/Cr mirror at elevated temperature using soft X-ray reflectivity.

Authors:  Mohammed H Modi; Shruti Gupta; Praveen K Yadav; Rajkumar Gupta; Aniruddha Bose; Chandrachur Mukherjee; Philippe Jonnard; Mourad Idir
Journal:  J Synchrotron Radiat       Date:  2022-05-25       Impact factor: 2.557

6.  Fast X-ray microdiffraction techniques for studying irreversible transformations in materials.

Authors:  Stephen T Kelly; Jonathan C Trenkle; Lucas J Koerner; Sara C Barron; Nöel Walker; Philippe O Pouliquen; Mark W Tate; Sol M Gruner; Eric M Dufresne; Timothy P Weihs; Todd C Hufnagel
Journal:  J Synchrotron Radiat       Date:  2011-03-16       Impact factor: 2.616

7.  A middle energy-bandwidth X-ray monochromator for high-flux synchrotron diffraction: revisiting asymmetrically cut silicon crystals.

Authors:  Hiroo Tajiri; Hiroshi Yamazaki; Haruhiko Ohashi; Shunji Goto; Osami Sakata; Tetsuya Ishikawa
Journal:  J Synchrotron Radiat       Date:  2019-04-17       Impact factor: 2.616

8.  Optimizing the energy bandwidth for transmission full-field X-ray microscopy experiments.

Authors:  Malte Storm; Florian Döring; Shashidhara Marathe; Silvia Cipiccia; Christian David; Christoph Rau
Journal:  J Synchrotron Radiat       Date:  2022-01-01       Impact factor: 2.616

  8 in total

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