Literature DB >> 15760232

Microwave-assisted synthesis of isonitriles: a general simple methodology.

Andrea Porcheddu1, Giampaolo Giacomelli, Margherita Salaris.   

Abstract

[reaction: see text] A facile conversion of formamides to isonitriles under very mild conditions and microwave irradiation is described. This simple and efficient method has been applied for the synthesis of both aliphatic and aromatic isonitriles in high yields.

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Year:  2005        PMID： 15760232     DOI： 10.1021/jo047924f

Source DB:  PubMed          Journal:  J Org Chem        ISSN： 0022-3263            Impact factor:   4.354


  9 in total

Review 1.  Controlled microwave heating in modern organic synthesis: highlights from the 2004-2008 literature.

Authors:  C Oliver Kappe; Doris Dallinger
Journal:  Mol Divers       Date:  2009-04-21       Impact factor: 2.943

2.  Complementary isonitrile-based multicomponent reactions for the synthesis of diversified cytotoxic hemiasterlin analogues.

Authors:  Giordano Lesma; Ivan Bassanini; Roberta Bortolozzi; Chiara Colletto; Ruoli Bai; Ernest Hamel; Fiorella Meneghetti; Giulia Rainoldi; Mattia Stucchi; Alessandro Sacchetti; Alessandra Silvani; Giampietro Viola
Journal:  Org Biomol Chem       Date:  2015-10-15       Impact factor: 3.876

3.  Enhancing the scope of the Diels-Alder reaction through isonitrile chemistry: emergence of a new class of acyl-activated dienophiles.

Authors:  Steven D Townsend; Xiangyang Wu; Samuel J Danishefsky
Journal:  J Am Chem Soc       Date:  2012-06-18       Impact factor: 15.419

4.  Welwitindolinone C synthetic studies. Construction of the welwitindolinone carbon skeleton via a transannular nitrone cycloaddition.

Authors:  David B Freeman; Alexandra A Holubec; Matthew W Weiss; Julie A Dixon; Akio Kakefuda; Masami Ohtsuka; Munenori Inoue; Rishi G Vaswani; Hidenori Ohki; Brian D Doan; Sarah E Reisman; Brian M Stoltz; Joshua J Day; Ran N Tao; Noah A Dieterich; John L Wood
Journal:  Tetrahedron       Date:  2010-08-14       Impact factor: 2.457

5.  The Michael addition of indoles and pyrrole to alpha-, beta-unsaturated ketones and double-conjugate 1,4-addition of indoles to symmetric enones promoted by pulverization-activation method and Thia-Michael addition catalyzed by wet cyanuric chloride.

Authors:  Ramin Ghorbani-Vaghei; Hojat Veisi
Journal:  Mol Divers       Date:  2009-08-07       Impact factor: 2.943

6.  Characterization, optimization, and in vitro evaluation of Technetium-99m-labeled niosomes.

Authors:  Leanne De Silva; Ju-Yen Fu; Thet Thet Htar; Saravanan Muniyandy; Azahari Kasbollah; Wan Hamirul Bahrin Wan Kamal; Lay-Hong Chuah
Journal:  Int J Nanomedicine       Date:  2019-02-12

7.  A trustworthy mechanochemical route to isocyanides.

Authors:  Francesco Basoccu; Federico Cuccu; Federico Casti; Rita Mocci; Claudia Fattuoni; Andrea Porcheddu
Journal:  Beilstein J Org Chem       Date:  2022-06-22       Impact factor: 2.544

8.  N-Formylsaccharin: A Sweet(able) Formylating Agent in Mechanochemistry.

Authors:  Federico Cuccu; Francesco Basoccu; Claudia Fattuoni; Andrea Porcheddu
Journal:  Molecules       Date:  2022-08-25       Impact factor: 4.927

9.  One-pot synthesis of 2-substituted 4H-3,1-benzoxazin-4-one derivatives under mild conditions using iminium cation from cyanuric chloride/dimethylformamide as a cyclizing agent.

Authors:  Mehdi Shariat; Mohd Wahid Samsudin; Zuriati Zakaria
Journal:  Chem Cent J       Date:  2013-03-27       Impact factor: 4.215
  9 in total

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