Literature DB >> 15729818

Analysis of flame retardant additives in polymer fractions of waste of electric and electronic equipment (WEEE) by means of HPLC-UV/MS and GPC-HPLC-UV.

Martin Schlummer1, Fritz Brandl, Andreas Mäurer, Rudi van Eldik.   

Abstract

An HPLC-UV/MS method has been developed to identify and quantify flame retardants in post-consumer plastics from waste of electric and electronic equipment (WEEE). Atmospheric pressure chemical ionisation spectra of 15 brominated and phosphate-based flame retardants were recorded and interpreted. The method was applied to detect flame retardant additives in polymer extracts obtained from pressurised liquid extraction of solid polymers. In addition, a screening method was developed for soluble styrene polymers to isolate a flame retardant fraction through the application of gel permeation chromatography (GPC). This fraction was transferred to an online-coupled HPLC column and detected by UV spectroscopy, which allowed a reliable qualitative and quantitative analysis of brominated flame retardants in the polymer solutions.

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Year:  2005        PMID： 15729818     DOI： 10.1016/j.chroma.2004.12.016

Source DB:  PubMed          Journal:  J Chromatogr A        ISSN： 0021-9673            Impact factor:   4.759


  5 in total

1.  Post-combustion syntheses of PCDD/F and PBDD/F from halogen-rich fuel is suppressed by a pebble heater technology.

Authors:  Martin Schlummer; Andreas Mäurer; Rudi van Eldik; Peter Quicker; Werner Fischer; Martin Faulstich
Journal:  Environ Sci Pollut Res Int       Date:  2007-09       Impact factor: 4.223

2.  Optimization and development of analytical methods for the determination of new brominated flame retardants and polybrominated diphenyl ethers in sediments and suspended particulate matter.

Authors:  P López; S A Brandsma; P E G Leonards; J de Boer
Journal:  Anal Bioanal Chem       Date:  2011-03-03       Impact factor: 4.142

Review 3.  Opportunities and challenges for the application of post-consumer plastic waste pyrolysis oils as steam cracker feedstocks: To decontaminate or not to decontaminate?

Authors:  Marvin Kusenberg; Andreas Eschenbacher; Marko R Djokic; Azd Zayoud; Kim Ragaert; Steven De Meester; Kevin M Van Geem
Journal:  Waste Manag       Date:  2021-12-03       Impact factor: 7.145

4.  Evidence of waste electrical and electronic equipment (WEEE) relevant substances in polymeric food-contact articles sold on the European market.

Authors:  Franky Puype; Jiří Samsonek; Jan Knoop; Marion Egelkraut-Holtus; Markus Ortlieb
Journal:  Food Addit Contam Part A Chem Anal Control Expo Risk Assess       Date:  2015-02-17

5.  Artificial photosynthesis of oxalate and oxalate-based polymer by a photovoltaic reactor.

Authors:  Guangzai Nong; Shan Chen; Yuanjin Xu; Lijie Huang; Qingsong Zou; Shiqiang Li; Haitao Mo; Pingchuan Zhu; Weijian Cen; Shuangfei Wang
Journal:  Sci Rep       Date:  2014-01-06       Impact factor: 4.379
  5 in total

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