Literature DB >> 15481471

Chlorotrimethylsilane, a reagent for the direct quantitative analysis of fats and oils present in vegetable and meat samples.

Jordi Eras1, Javier Ferran, Belén Perpiña, Ramon Canela.   

Abstract

Acylglycerides present in oil seeds and meat can be transformed into volatile fatty esters using chlorotrimethylsilane (CTMS) and 1-pentanol as reagents. The volatile esters can then be analysed by GC. The method is quantitative and involves only minor sample manipulation. It often permits major recoveries of the total saponifiable lipids present in solid samples. A 40 min reaction time is enough to ensure the total conversion of saponifiable lipids to the corresponding FAPEs.

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Year:  2004        PMID: 15481471     DOI: 10.1016/j.chroma.2004.07.014

Source DB:  PubMed          Journal:  J Chromatogr A        ISSN: 0021-9673            Impact factor:   4.759


  1 in total

1.  A simple and fast method for metabolomic analysis by gas liquid chromatography-mass spectrometry.

Authors:  Diana Cosovanu; Montserrat Llovera; Gemma Villorbina; Ramon Canela-Garayoa; Jordi Eras
Journal:  Metabolomics       Date:  2021-02-06       Impact factor: 4.290

  1 in total

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