Literature DB >> 12504387

A simple method for preparation of D-rhamnose.

Michael Ramm1, Martina Lobe, Matthias Hamburger.   

Abstract

A rapid procedure for the preparation of D-rhamnose from bacterial lipopolysaccharide (LPS) has been developed. It involves purification of LPS from Pseudomonas syringae pv. phaseolicola by phenol extraction and hydrophobic interaction chromatography (HIC), followed by mild hydrolysis and cleavage of the O-antigen into D-fucose and D-rhamnose. The monosaccharides were separated by column chromatography, and D-rhamnose recovered after filtration over Sephadex-LH 20.

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Year:  2003        PMID： 12504387     DOI： 10.1016/s0008-6215(02)00353-1

Source DB:  PubMed          Journal:  Carbohydr Res        ISSN： 0008-6215            Impact factor:   2.104


  5 in total

1.  On the nitrile effect in L-rhamnopyranosylation.

Authors:  David Crich; Mitesh Patel
Journal:  Carbohydr Res       Date:  2006-04-27       Impact factor: 2.104

2.  4,6-O-[1-cyano-2-(2-iodophenyl)ethylidene] acetals. improved second-generation acetals for the stereoselective formation of beta-D-mannopyranosides and regioselective reductive radical fragmentation to beta-D-rhamnopyranosides. scope and limitations.

Authors:  David Crich; Albert A Bowers
Journal:  J Org Chem       Date:  2006-04-28       Impact factor: 4.354

3.  Stereocontrolled synthesis of the D- and L-glycero-beta-D-manno-heptopyranosides and their 6-deoxy analogues. Synthesis of methyl alpha-l-rhamno-pyranosyl-(1-->3)-D-glycero-beta-D-manno-heptopyranosyl- (1-->3)-6-deoxy-glycero-beta-D-manno-heptopyranosyl-(1-->4)-alpha-L- rhamno-pyranoside, a tetrasaccharide subunit of the lipopolysaccharide from Plesimonas shigelloides.

Authors:  David Crich; Abhisek Banerjee
Journal:  J Am Chem Soc       Date:  2006-06-21       Impact factor: 15.419

4.  Lectin-like bacteriocins from Pseudomonas spp. utilise D-rhamnose containing lipopolysaccharide as a cellular receptor.

Authors:  Laura C McCaughey; Rhys Grinter; Inokentijs Josts; Aleksander W Roszak; Kai I Waløen; Richard J Cogdell; Joel Milner; Tom Evans; Sharon Kelly; Nicholas P Tucker; Olwyn Byron; Brian Smith; Daniel Walker
Journal:  PLoS Pathog       Date:  2014-02-06       Impact factor: 6.823

5.  Discovery, characterization and in vivo activity of pyocin SD2, a protein antibiotic from Pseudomonas aeruginosa.

Authors:  Laura C McCaughey; Inokentijs Josts; Rhys Grinter; Paul White; Olwyn Byron; Nicholas P Tucker; Jacqueline M Matthews; Colin Kleanthous; Cynthia B Whitchurch; Daniel Walker
Journal:  Biochem J       Date:  2016-06-01       Impact factor: 3.857
  5 in total

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