Literature DB >> 1218089

Characterization by gas-liquid chromatography-mass spectrometry and proton-magnetic-resonance spectroscopy of pertrimethylsilyl methyl glycosides obtained in the methanolysis of glycoproteins and glycopeptides.

J P Kamerling, G J Gerwig, J F Vliegenthart, J R Clamp.   

Abstract

The quantitative analysis by gas chromatography of monosaccharides present in glycoproteins and glycopeptides using methanolysis, followed by re-N-acetylation and trimethylsilylation, gives rise to several peaks for each monosaccharide. The identity of these peaks for xylose, fucose, mannose, galactose, glucose, N-acetylglucosamine, N-acetylgalactosamine and N-acetylneuraminic acid was established for alpha- and beta-methyl pyranosides and furanosides by combined g.l.c.-mass spectrometry and proton-magnetic-resonance spectroscopy. These data provide for the unambiguous interpretation of the gas chromatograms obtained in the application of this g.l.c. method, and supply basic information for the further application of mass spectrometry in this field.

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Year:  1975        PMID： 1218089      PMCID： PMC1172395          DOI： 10.1042/bj1510491

Source DB:  PubMed          Journal:  Biochem J        ISSN： 0264-6021            Impact factor:   3.857


  8 in total

Review 1.  CHEMISTRY OF THE CARBOHYDRATES.

Authors:  R U LEMIEUX; R LINEBACK
Journal:  Annu Rev Biochem       Date:  1963       Impact factor: 23.643

2.  Identification of O-cetylated N-acylneuraminic acids by mass spectrometry.

Authors:  J P Kamerling; J F Vliegenthart
Journal:  Carbohydr Res       Date:  1975-05       Impact factor: 2.104

3.  Occurrence of a galactofuranose disaccharide in immunoadjuvant fractions of Mycobacterium tuberculosis (Cell walls and wax D).

Authors:  E Vilkas; C Amar; J Markovits; J F Vliegenthart; J P Kamerling
Journal:  Biochim Biophys Acta       Date:  1973-02-28

4.  Configuration of the ketosidic bond of sialic acid.

Authors:  R K Yu; R Ledeen
Journal:  J Biol Chem       Date:  1969-03-10       Impact factor: 5.157

Review 5.  The determination of carbohydrate in biological materials by gas-liquid chromatography.

Authors:  J R Clamp; T Bhatti; R E Chambers
Journal:  Methods Biochem Anal       Date:  1971

6.  An evaluation of methanolysis for thin-layer chromatographic analysis of the monosaccharides in an immunologically active polysaccharide-peptide complex.

Authors:  Y Nozawa; H Uesaka; H Suzuki; Y Ito
Journal:  J Chromatogr       Date:  1969-09-23

Review 7.  Analysis of glycoproteins.

Authors:  J R Clamp
Journal:  Biochem Soc Symp       Date:  1974

8.  An assessment of methanolysis and other factors used in the analysis of carbohydrate-containing materials.

Authors:  R E Chambers; J R Clamp
Journal:  Biochem J       Date:  1971-12       Impact factor: 3.857
  8 in total
  71 in total

1.  Novel storage products in human beta-mannosidosis.

Authors:  C H Hokke; M Duran; L Dorland; J van Pelt; F J van Sprang
Journal:  J Inherit Metab Dis       Date:  1990       Impact factor: 4.982

2.  The oligomeric structure of rat and human gastric mucins.

Authors:  J Dekker; P H Aelmans; G J Strous
Journal:  Biochem J       Date:  1991-07-15       Impact factor: 3.857

3.  Minimal oligosaccharide structures required for induction of immune responses against meningococcal immunotype L1, L2, and L3,7,9 lipopolysaccharides determined by using synthetic oligosaccharide-protein conjugates.

Authors:  A F Verheul; G J Boons; G A Van der Marel; J H Van Boom; H J Jennings; H Snippe; J Verhoef; P Hoogerhout; J T Poolman
Journal:  Infect Immun       Date:  1991-10       Impact factor: 3.441

4.  Glycosylation of human fetal mucins: a similar repertoire of O-glycans along the intestinal tract.

Authors:  Catherine Robbe-Masselot; Emmanuel Maes; Monique Rousset; Jean-Claude Michalski; Calliope Capon
Journal:  Glycoconj J       Date:  2008-09-20       Impact factor: 2.916

5.  Structural analysis of a new series of oligosaccharide-alditols released by reductive beta-elimination from oviducal mucins of Rana utricularia.

Authors:  W Morelle; G Strecker
Journal:  Biochem J       Date:  1998-02-15       Impact factor: 3.857

6.  Self-aggregation of Cryptococcus neoformans capsular glucuronoxylomannan is dependent on divalent cations.

Authors:  Leonardo Nimrichter; Susana Frases; Leonardo P Cinelli; Nathan B Viana; Antonio Nakouzi; Luiz R Travassos; Arturo Casadevall; Marcio L Rodrigues
Journal:  Eukaryot Cell       Date:  2007-06-15

7.  Chemical and immunological characterization of the extracellular galactomannan of Aspergillus fumigatus.

Authors:  J P Latgé; H Kobayashi; J P Debeaupuis; M Diaquin; J Sarfati; J M Wieruszeski; E Parra; J P Bouchara; B Fournet
Journal:  Infect Immun       Date:  1994-12       Impact factor: 3.441

8.  Epitope specificity of rabbit immunoglobulin G (IgG) elicited by pneumococcal type 23F synthetic oligosaccharide- and native polysaccharide-protein conjugate vaccines: comparison with human anti-polysaccharide 23F IgG.

Authors:  E Alonso de Velasco; A F Verheul; A M van Steijn; H A Dekker; R G Feldman; I M Fernández; J P Kamerling; J F Vliegenthart; J Verhoef; H Snippe
Journal:  Infect Immun       Date:  1994-03       Impact factor: 3.441

9.  Nonionic block polymer surfactants modulate the humoral immune response against Streptococcus pneumoniae-derived hexasaccharide-protein conjugates.

Authors:  G J Zigterman; K Schotanus; E B Ernste; G J Van Dam; M Jansze; H Snippe; J M Willers
Journal:  Infect Immun       Date:  1989-09       Impact factor: 3.441

10.  Immunogenic properties in mice of hexasaccharide from the capsular polysaccharide of Streptococcus pneumoniae type 3.

Authors:  H Snippe; A J van Houte; J E van Dam; M J De Reuver; M Jansze; J M Willers
Journal:  Infect Immun       Date:  1983-06       Impact factor: 3.441
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