Literature DB >> 12126436

An improved protocol for the preparation of 3-pyridyl- and some arylboronic acids.

Wenjie Li1, Dorian P Nelson, Mark S Jensen, R Scott Hoerrner, Dongwei Cai, Robert D Larsen, Paul J Reider.   

Abstract

3-Pyridylboronic acid was prepared in high yield and bulk quantity from 3-bromopyridine via a protocol of lithium-halogen exchange and "in situ quench". This technique was further studied and evaluated on other aryl halides in the preparation of arylboronic acids.

Entities:  

Year:  2002        PMID： 12126436     DOI： 10.1021/jo025792p

Source DB:  PubMed          Journal:  J Org Chem        ISSN： 0022-3263            Impact factor:   4.354


  18 in total

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6.  Palladium-catalyzed, direct boronic acid synthesis from aryl chlorides: a simplified route to diverse boronate ester derivatives.

Authors:  Gary A Molander; Sarah L J Trice; Spencer D Dreher
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8.  Synthesis of sulfonamide- and sulfonyl-phenylboronic acid-modified silica phases for boronate affinity chromatography at physiological pH.

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10.  Discovery of the Selective CYP17A1 Lyase Inhibitor BMS-351 for the Treatment of Prostate Cancer.

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Journal:  ACS Med Chem Lett       Date:  2015-12-02       Impact factor: 4.345
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