Literature DB >> 11975492

Evaluation of glucoiberin reference material from Iberis amara by spectroscopic fingerprinting.

Birgit Jaki1, Otto Sticher, Markus Veit, Roland Fröhlich, Guido F Pauli.   

Abstract

Increasing worldwide regulations require increased efforts toward validation of analytical and pharmacological reference materials. A detailed survey of glucoiberin, a prototype lead constituent of therapeutic value, using 1D/2D NMR, MS, and X-ray spectroscopy provided precise phytochemical data for structure assignment. Quantitative reference validation was achieved by the recently proposed qNMR method.

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Year:  2002        PMID: 11975492     DOI: 10.1021/np0100800

Source DB:  PubMed          Journal:  J Nat Prod        ISSN: 0163-3864            Impact factor:   4.050


  4 in total

1.  Selective quantification by 2D HSQC0 spectroscopy of thiocoraline in an extract from a sponge-derived Verrucosispora sp.

Authors:  Kaifeng Hu; Thomas P Wyche; Tim S Bugni; John L Markley
Journal:  J Nat Prod       Date:  2011-09-16       Impact factor: 4.050

2.  Dynamic residual complexity of natural products by qHNMR: solution stability of desmethylxanthohumol.

Authors:  Shao-Nong Chen; David C Lankin; Lucas R Chadwick; Birgit U Jaki; Guido F Pauli
Journal:  Planta Med       Date:  2009-01-14       Impact factor: 3.352

Review 3.  Importance of purity evaluation and the potential of quantitative ¹H NMR as a purity assay.

Authors:  Guido F Pauli; Shao-Nong Chen; Charlotte Simmler; David C Lankin; Tanja Gödecke; Birgit U Jaki; J Brent Friesen; James B McAlpine; José G Napolitano
Journal:  J Med Chem       Date:  2014-10-08       Impact factor: 7.446

Review 4.  Glucosinolates: Natural Occurrence, Biosynthesis, Accessibility, Isolation, Structures, and Biological Activities.

Authors:  V P Thinh Nguyen; Jon Stewart; Michel Lopez; Irina Ioannou; Florent Allais
Journal:  Molecules       Date:  2020-10-03       Impact factor: 4.411

  4 in total

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