Literature DB >> 1178524

Thioacyl esters of nucleotides: synthesis of 3'(2')-O-thiobenzoyl nucleoside 5'-phosphates.

A V Azhayev, A A Krayevsky, V L Florentiev, M K Kukhanova, B P Gottikh.   

Abstract

The synthesis of 3'(2')-O-thiobenzoyl nucleoside 5'-phosphates based on the condensation of N-(thiobenzoyl)-imidazole with nucleside 5'-phosphates was carried out. The UV absorption spectra, CD spectra, PMR spectra and chromatographic and electrophoretic characteristics of synthesized compounds were obtained. By means of PMR it was shown that the 2':3' isomer ratio in water at ambient temperature is about 2:3.

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Year:  1975        PMID: 1178524      PMCID: PMC343514          DOI: 10.1093/nar/2.9.1433

Source DB:  PubMed          Journal:  Nucleic Acids Res        ISSN: 0305-1048            Impact factor:   16.971


  1 in total

1.  The synthesis of oligoribonucleotides. IV. Preparation of dinucleoside phosphates from 2',5'-protected ribonucleoside derivatives.

Authors:  B E Griffin; M Jarman; C B Reese
Journal:  Tetrahedron       Date:  1968-01       Impact factor: 2.457

  1 in total

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