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Literature DB >> 11348247

A convenient method for the efficient removal of ruthenium byproducts generated during olefin metathesis reactions.

Abstract

[reaction in text] An efficient method for removing ruthenium byproducts generated during olefin metathesis reactions with Grubbs catalysts is described. Treatment of the crude reaction products with triphenylphosphine oxide or dimethyl sulfoxide, followed by filtration through silica gel, was found to be a practical and effective method to remove colored ruthenium byproducts.

Entities: Chemical

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Year: 2001 PMID： 11348247 DOI： 10.1021/ol010045k

Source DB: PubMed Journal: Org Lett ISSN： 1523-7052 Impact factor: 6.005

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Cited

14 in total

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Authors: Prakash B Palde; Leslie O Ofori; Peter C Gareiss; Jaclyn Lerea; Benjamin L Miller
Journal: J Med Chem Date: 2010-08-26 Impact factor: 7.446

2. Stereocontrolled Synthesis of a Potential Transition-State Inhibitor of the Salicylate Synthase MbtI from Mycobacterium tuberculosis.

Authors: Zheng Liu; Feng Liu; Courtney C Aldrich
Journal: J Org Chem Date: 2015-06-16 Impact factor: 4.354

3. Synthesis of Diverse Heterocyclic Scaffolds via Tandem Additions to Imine Derivatives and Ring-Forming Reactions.

Authors: James D Sunderhaus; Chris Dockendorff; Stephen F Martin
Journal: Tetrahedron Date: 2009-09-15 Impact factor: 2.457

4. Heterogeneous Removal of Water-Soluble Ruthenium Olefin Metathesis Catalyst from Aqueous Media Via Host-Guest Interaction.

Authors: Cheoljae Kim; Hoyong Chung
Journal: J Vis Exp Date: 2018-08-23 Impact factor: 1.355

5. Catalytic living ring-opening metathesis polymerization.

Authors: Amit A Nagarkar; Andreas F M Kilbinger
Journal: Nat Chem Date: 2015-08-10 Impact factor: 24.427

6. A convenient method to remove ruthenium byproducts from olefin metathesis reactions using polymer-bound triphenylphosphine oxide (TPPO).

Authors: KyoungLang Haack; Yu Mi Ahn; Gunda I Georg
Journal: Mol Divers Date: 2005 Impact factor: 2.943

A convenient method for the efficient removal of ruthenium byproducts generated during olefin metathesis reactions.

1. Strategies for recognition of stem-loop RNA structures by synthetic ligands: application to the HIV-1 frameshift stimulatory sequence.

2. Stereocontrolled Synthesis of a Potential Transition-State Inhibitor of the Salicylate Synthase MbtI from Mycobacterium tuberculosis.

3. Synthesis of Diverse Heterocyclic Scaffolds via Tandem Additions to Imine Derivatives and Ring-Forming Reactions.

4. Heterogeneous Removal of Water-Soluble Ruthenium Olefin Metathesis Catalyst from Aqueous Media Via Host-Guest Interaction.

5. Catalytic living ring-opening metathesis polymerization.

6. A convenient method to remove ruthenium byproducts from olefin metathesis reactions using polymer-bound triphenylphosphine oxide (TPPO).

7. Synthesis of orthogonally reactive FK506 derivatives via olefin cross metathesis.

8. Efficient removal of ruthenium byproducts from olefin metathesis products by simple aqueous extraction.

9. A fluorous-tagged linker from which small molecules are released by ring-closing metathesis.

10. Highly Efficient Biobased Synthesis of Acrylic Acid.