Literature DB >> 11269588

High-resolution analysis of polyprenols by supercritical fluid chromatography.

T Bamba1, W Fukasaki, S Kajiyama, K Ute, T Kitayama, A Kobayashi.   

Abstract

A high-resolution analysis of polyprenol mixtures was achieved by supercritical fluid chromatography (SFC). The separation of polyprenols was examined on an octadecylsilane-packed column with liquid carbon dioxide as the mobile phase and ethanol as modifier. Using this chromatography system, the resolution of separation (Rs) between octadecaprenol (prenol 18) and nonadecaprenol (prenol 19) was two times higher than that using conventional reversed-phase high-performance liquid chromatography. Our SFC technique allows the advantage of baseline separation of polyprenol samples containing hydrophobic components such as terpenes or fatty acids that are unfavorable for good separation. This method is very useful for the analysis of structurally close polyprenol analogues of rubber plant metabolites.

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Year:  2001        PMID: 11269588     DOI: 10.1016/s0021-9673(00)01250-4

Source DB:  PubMed          Journal:  J Chromatogr A        ISSN: 0021-9673            Impact factor:   4.759


  3 in total

1.  The occurrence of geometric polyprenol isomers in the rubber-producing plant, Eucommia ulmoides Oliver.

Authors:  T Bamba; E Fukusaki; S Kajiyama; K Ute; T Kitayama; A Kobayashi
Journal:  Lipids       Date:  2001-07       Impact factor: 1.880

Review 2.  Lipidomics by Supercritical Fluid Chromatography.

Authors:  Laurent Laboureur; Mario Ollero; David Touboul
Journal:  Int J Mol Sci       Date:  2015-06-17       Impact factor: 5.923

Review 3.  Advances of supercritical fluid chromatography in lipid profiling.

Authors:  Yang Yang; Yanshan Liang; Jina Yang; Fengying Ye; Ting Zhou; Li Gongke
Journal:  J Pharm Anal       Date:  2018-11-17
  3 in total

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