Literature DB >> 10891201

A Simple One-Pot Procedure for the Direct Conversion of Alcohols to Azides via Phosphate Activation.

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Abstract

A one-pot procedure was developed to prepare efficiently alkyl azides from alkanols using bis(2,4-dichlorophenyl) phosphate activation. 4-(Dimethylamino)pyridine was used as a base, and phosphorylpyridinium azide is believed to be the activating agent under this condition.

Entities:  

Year:  2000        PMID： 10891201     DOI： 10.1021/ol0060376

Source DB:  PubMed          Journal:  Org Lett        ISSN： 1523-7052            Impact factor:   6.005


  4 in total

1.  Design, synthesis, docking, and biological evaluation of novel diazide-containing isoxazole- and pyrazole-based histone deacetylase probes.

Authors:  Raghupathi Neelarapu; Denise L Holzle; Subash Velaparthi; He Bai; Michael Brunsteiner; Sylvie Y Blond; Pavel A Petukhov
Journal:  J Med Chem       Date:  2011-06-02       Impact factor: 7.446

2.  SulfoxFluor-enabled deoxyazidation of alcohols with NaN3.

Authors:  Junkai Guo; Xiu Wang; Chuanfa Ni; Xiaolong Wan; Jinbo Hu
Journal:  Nat Commun       Date:  2022-05-18       Impact factor: 17.694

3.  Farnesyl diphosphate analogues with omega-bioorthogonal azide and alkyne functional groups for protein farnesyl transferase-catalyzed ligation reactions.

Authors:  Guillermo R Labadie; Rajesh Viswanathan; C Dale Poulter
Journal:  J Org Chem       Date:  2007-11-03       Impact factor: 4.354

4.  In situ generation of N-unsubstituted imines from alkyl azides and their applications for imine transfer via copper catalysis.

Authors:  Lu Hu; Yahu A Liu; Xuebin Liao
Journal:  Sci Adv       Date:  2017-08-09       Impact factor: 14.136
  4 in total

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